{"id":123964,"date":"2018-02-04T06:30:59","date_gmt":"2018-02-03T22:30:59","guid":{"rendered":"\/\/m.iemloyee.com\/?p=123964"},"modified":"2018-03-01T10:16:20","modified_gmt":"2018-03-01T02:16:20","slug":"macromolecules%ef%bc%9a%e5%9c%a8%e8%81%9a%e5%90%88%e8%af%b1%e5%af%bc%e8%87%aa%e7%bb%84%e8%a3%85%e8%bf%87%e7%a8%8b%e4%b8%ad%e9%80%9a%e8%bf%87%e6%8b%93%e6%89%91%e5%b7%a5%e7%a8%8b%e6%8e%a7%e5%88%b6","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=123964","title":{"rendered":"Macromolecules\uff1a\u5728\u805a\u5408\u8bf1\u5bfc\u81ea\u7ec4\u88c5\u8fc7\u7a0b\u4e2d\u901a\u8fc7\u62d3\u6251\u5de5\u7a0b\u63a7\u5236\u4e24\u4eb2\u6027\u805a\u5408\u7269\u56ca\u6ce1\u5c3a\u5bf8"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u805a\u5408\u7269\u56ca\u6ce1\u662f\u4e00\u7c7b\u7531\u4e24\u4eb2\u6027\u5171\u805a\u7269\u7ec4\u6210\u7684\u81ea\u7ec4\u88c5\u53cc\u5c42\u819c\uff0c\u5177\u6709\u4e0e\u7ec6\u80de\u819c\u76f8\u4f3c\u7684\u7ed3\u6784\u7279\u5f81\uff0c\u81ea\u51fa\u73b0\u4ee5\u6765\u5df2\u5f15\u8d77\u4e86\u4eba\u4eec\u7684\u6781\u5927\u5173\u6ce8\u3002\u4e0e\u5176\u5c0f\u5206\u5b50\u5bf9\u5e94\u7269\u8102\u8d28\u4f53\u76f8\u6bd4\uff0c\u805a\u5408\u7269\u56ca\u6ce1\u5728\u6781\u7a00\u65f6\u8868\u73b0\u51fa\u4f18\u5f02\u7684\u7a33\u5b9a\u6027\uff1b\u6b64\u5916\uff0c\u805a\u5408\u7269\u56ca\u6ce1\u7684\u5c3a\u5bf8\u3001\u6e17\u900f\u6027\u548c\u8868\u9762\u6027\u80fd\u7b49\u5747\u53ef\u65b9\u4fbf\u8c03\u6574\u5e76\u4f7f\u5176\u9002\u5e94\u751f\u7269\u4f53\u5185\u73af\u5883\u7684\u8981\u6c42\u3002\u56e0\u6b64\uff0c\u805a\u5408\u7269\u56ca\u6ce1\u5728\u533b\u836f\u6750\u6599\u9886\u57df\u5177\u6709\u4e00\u5b9a\u6f5c\u529b\uff0c\u6709\u671b\u5e94\u7528\u5230\u836f\u7269\u6216\u57fa\u56e0\u8f7d\u4f53\u3001\u7eb3\u7c73\u53cd\u5e94\u5668\u3001\u4eba\u9020\u7ec6\u80de\u5668\u7b49\u7684\u7814\u53d1\u4e2d\u3002<\/p>\n

\u805a\u5408\u7269\u56ca\u6ce1\u901a\u5e38\u662f\u901a\u8fc7\u7eb3\u7c73\u6c89\u6dc0\u6216\u8584\u819c\u6c34\u5316\u6280\u672f\u7531\u4e24\u4eb2\u6027\u5171\u805a\u7269\u81ea\u7ec4\u88c5\u5236\u5907\u7684\uff0c\u4f46\u4f20\u7edf\u7684\u5236\u5907\u65b9\u6cd5\u5f80\u5f80\u53d7\u5230\u4f4e\u56fa\u4f53\u542b\u91cf\u548c\u590d\u6742\u52a8\u529b\u5b66\u7b49\u7f3a\u9677\u7684\u5f71\u54cd\u3002\u6700\u8fd1\uff0c\u201c\u805a\u5408\u8bf1\u5bfc\u81ea\u7ec4\u88c5\uff08PISA\uff09\u201d\u7684\u65b0\u65b9\u6cd5\u6210\u4e3a\u5b9e\u73b0\u805a\u5408\u7269\u81ea\u7ec4\u88c5\u7684\u6709\u6548\u7b56\u7565\uff0c\u8be5\u65b9\u6cd5\u5229\u7528\u4eb2\u6eb6\u5242\u805a\u5408\u7269\u94fe\u5f15\u53d1\u618e\u6eb6\u5242\u5d4c\u6bb5\u7684\u589e\u957f\u3002\u968f\u7740\u618e\u6eb6\u5242\u5d4c\u6bb5\u7684\u751f\u957f\uff0c\u4e24\u4eb2\u6027\u5d4c\u6bb5\u5171\u805a\u7269\u539f\u4f4d\u7f14\u5408\u6210\u7ec4\u88c5\u4f53\uff0c\u8fdb\u4e00\u6b65\u91cd\u7ec4\u4e3a\u5176\u4ed6\u5f62\u6001\uff0c\u5982\u8815\u866b\u72b6\u7684\u80f6\u675f\u548c\u56ca\u6ce1\u7b49\u3002PISA\u673a\u7406\u72ec\u7279\uff0c\u53ef\u901a\u8fc7\u7b80\u5355\u8c03\u8282\u805a\u5408\u914d\u65b9\u7684\u65b9\u6cd5\u4f7f\u76ee\u6807\u9ad8\u5206\u5b50\u5728\u9ad8\u56fa\u542b\u91cf\u4e0b\u5b9e\u73b0\u81ea\u7ec4\u88c5\u3002\u7136\u800c\uff0cPISA\u5bf9\u805a\u5408\u7269\u81ea\u7ec4\u88c5\u7eb3\u7c73\u7ed3\u6784\u7684\u63a7\u5236\u80fd\u529b\u5341\u5206\u6709\u9650\u3002\u4f8b\u5982\uff0c\u901a\u5e38PISA\u5236\u5907\u5f97\u5230\u7684\u56ca\u6ce1\u5c3a\u5bf8\u96be\u4ee5\u901a\u8fc7\u7b80\u5355\u7684\u618e\u6eb6\u5242\u94fe\u6bb5\u7684\u957f\u5ea6\u8c03\u8282\u5b9e\u73b0\u8c03\u63a7\u3002<\/p>\n

\u76ee\u524d\u4e3a\u6b62\uff0c\u5173\u4e8ePISA\u8c03\u63a7\u805a\u5408\u7269\u56ca\u6ce1\u5c3a\u5bf8\u7684\u62a5\u9053\u8f83\u5c11\u3002D\u2019 Agosto\u7b49\u4eba\u7814\u7a76\u4e86\u4eb2\u6c34\u62d3\u6251\u7ed3\u6784\u5bf9\u805a\u5408\u7269\u7ec4\u88c5\u4f53\u5f62\u8c8c\u7684\u5f71\u54cd\uff0c\u8fd9\u9879\u5f00\u521b\u6027\u7814\u7a76\u8868\u660e\u805a\u5408\u7269\u62d3\u6251\u7ed3\u6784\u5bf9\u805a\u5408\u7269\u7ec4\u88c5\u4f53\u7684\u5c3a\u5bf8\u53ca\u5f62\u8c8c\u7684\u91cd\u8981\u6027\uff0c\u4f46\u8be5\u65b9\u6cd5\u53d7\u5230\u590d\u6742\u5408\u6210\u53ca\u4e0d\u660e\u786e\u7684\u8c03\u63a7\u673a\u7406\u7684\u9650\u5236\u3002\u56e0\u6b64\uff0c\u4eba\u4eec\u8feb\u5207\u9700\u8981\u63a2\u7d22\u4e00\u79cd\u5728\u56ca\u6ce1\u7eb3\u7c73\u7ed3\u6784\u4e0a\u5177\u6709\u666e\u904d\u9002\u7528\u6027\u548c\u8c03\u8282\u80fd\u529b\u7684\u7b80\u5355\u6a21\u5757\u5316\u65b9\u6cd5\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u6e05\u534e\u5927\u5b66\u8881\u91d1\u9896\u6559\u6388\u3001\u5371\u5ca9\u6559\u6388\u3001\u71d5\u7acb\u5510\u7814\u7a76\u5458\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09<\/strong>\u7b49\u4eba\u5728Macromolecule<\/strong>s\u671f\u520a\u4e0a\u53d1\u8868\u9898\u4e3a\u201cControlling Vesicular Size via Topological Engineering of Amphiphilic Polymer in Polymerization-Induced Self-Assembly<\/strong>\u201d\u7684\u6587\u7ae0\u3002\u6e05\u534e\u5927\u5b66\u5316\u5b66\u7cfb\u535a\u58eb\u751f\u970d\u731b\u548c\u5316\u5b66\u5de5\u7a0b\u7cfb\u535a\u58eb\u751f\u5f90\u5b50\u9633\u4e3a\u8bba\u6587\u7684\u5171\u540c\u7b2c\u4e00\u4f5c\u8005\u3002\u5728\u8be5\u6587\u4e2d\uff0c\u7814\u7a76\u4eba\u5458\u62a5\u9053\u4e86\u5229\u7528\u805a\u5408\u8bf1\u5bfc\u81ea\u7ec4\u88c5\uff08PISA\uff09\uff0c\u901a\u8fc7\u4e24\u4eb2\u6027\u5171\u805a\u7269\u618e\u6eb6\u5242\u5d4c\u6bb5\u7684\u62d3\u6251\u5de5\u7a0b\u5b9e\u73b0\u5c3a\u5bf8\u53ef\u8c03\u7684\u805a\u5408\u7269\u56ca\u6ce1\u5236\u5907\u7684\u65b9\u6cd5\u3002\u8bbe\u60f3\u6bcf\u79cd\u5355\u4f53\u90fd\u5177\u6709\u5176\u7279\u5b9a\u7684\u5206\u5b50\u4f53\u79ef\u548c\u5f62\u72b6\uff0c\u901a\u8fc7\u6539\u53d8\u4e24\u79cd\u5355\u4f53\u7684\u6295\u6599\u6bd4\u4eba\u4eec\u53ef\u7531RAFT\u5171\u805a\u53cd\u5e94\u7b80\u4fbf\u5730\u5236\u5907\u51fa\u5177\u6709\u4e0d\u540c\u62d3\u6251\u7ed3\u6784\u7684\u5171\u805a\u7269\u5206\u5b50\u3002\u5206\u5b50\u62d3\u6251\u7ed3\u6784\u7684\u5dee\u5f02\u53ef\u80fd\u4f7f\u4eba\u4eec\u83b7\u5f97\u5177\u6709\u53ef\u53d8\u94fe\u5806\u79ef\u5bc6\u5ea6\u548c\u53ef\u8c03\u7eb3\u7c73\u7ed3\u6784\u7684\u7ec4\u88c5\u4f53\u3002\u5728\u672c\u6587\u4e2d\uff0c\u7814\u7a76\u4eba\u5458\u62a5\u9053\u4e86\u4e00\u79cd\u901a\u7528\u548c\u6a21\u5757\u5316\u7b56\u7565\uff0c\u8be5\u7b56\u7565\u901a\u8fc7\u8c03\u8282\u758f\u6eb6\u5242\u5d4c\u6bb5\u7684\u62d3\u6251\u7ed3\u6784\u6765\u8c03\u8282\u56ca\u6ce1\u5927\u5c0f\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe1\uff1a\u8c03\u8282BzMA\u548cSMA\u7684\u6295\u6599\u6bd4\uff0c\u7531RAFT\u5206\u6563\u5171\u805a\u8c03\u8282\u56ca\u6ce1\u5c3a\u5bf8\u3002<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

\u56fe2\uff1a PDMA-b-P(BzMA-co-SMA)-42k-x (x = 0, 10, 20, 30, 50, 70, 90, 100)\u56ca\u6ce1\u7684TEM\u548cDLS\u8868\u5f81\u7ed3\u679c\u3002<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

\uff08a-h\uff09PDMA-b-P(BzMA-co-SMA)-42k-x\u56ca\u6ce1\u7684TEM\u56fe\u50cf\uff1a\uff08a\uff09x = 0\uff0c\uff08b\uff09x = 10\uff0c\uff08c\uff09x = 20\uff0c\uff08d\uff09x = 30\uff0c\uff08e\uff09x = 50\uff0c\uff08f\uff09x = 70\uff0c\uff08g\uff09x = 90\uff0c\uff08h\uff09x = 100\uff1b<\/p>\n

\uff08i\uff09PDMA-b-P(BzMA-co-SMA)-42k-x\u56ca\u6ce1\u7684\u5c3a\u5bf8\u7edf\u8ba1\u7ed3\u679c\u968fSMA\u8d28\u91cf\u5206\u6570\u53d8\u5316\u7684\u8d8b\u52bf\u56fe\uff1b<\/p>\n

\uff08j\uff09PDMA-b-P(BzMA-co-SMA)-42k-x\u56ca\u6ce1\u7684DLS\u66f2\u7ebf\uff1b<\/p>\n

\uff08k\uff09PDMA-b-P(BzMA-co-SMA)-42k-x\u56ca\u6ce1\u7684\u6570\u5747\u6c34\u5408\u52a8\u529b\u5b66\u76f4\u5f84\u968fSMA\u8d28\u91cf\u5206\u6570\u53d8\u5316\u7684\u8d8b\u52bf\u56fe\u3002<\/p>\n

\u56fe3\uff1aPDMA-b-P(BzMA-co-SMA)-88k-x(x = 0, 20, 40, 60, 80, 100)\u7684DLS\u548cTEM\u8868\u5f81\u7ed3\u679c\u3002<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

\uff08a\uff09PDMA-b-P(BzMA-co-SMA)-88k-x\u7684DLS\u66f2\u7ebf\uff1b<\/p>\n

\uff08b\uff09PDMA-b-P(BzMA-co-SMA)-88k-x\u7684\u6570\u5747\u6c34\u5408\u52a8\u529b\u5b66\u76f4\u5f84\u968fSMA\u8d28\u91cf\u5206\u6570\u53d8\u5316\u7684\u8d8b\u52bf\u56fe\uff1b<\/p>\n

\uff08c-h\uff09PDMA-b-P(BzMA-co-SMA)-88k-x\u7684TEM\u56fe\u50cf\uff1a\uff08c\uff09x = 0\uff0c\uff08d\uff09x =20\uff0c\uff08e\uff09x = 40\uff0c\uff08f\uff09x = 60\uff0c\uff08g\uff09x = 80\uff0c\uff08h\uff09x = 100\u3002<\/p>\n

\u56fe4\uff1a\u805a\u5408\u7269\u56ca\u6ce1\u5c3a\u5bf8\u53d8\u5316\u7684\u8ba1\u7b97\u673a\u6a21\u62df\u7ed3\u679c\u3002<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

\uff08a\uff09\u901a\u8fc7PISA\u5236\u5907\u5f97\u5230\u7684\u4eb2\u6c34\u6027PDMA\u5d4c\u6bb5\uff08\u7eff\u8272\uff09\u4e0e\u7531BzMA\uff08\u84dd\u8272\uff09\u548cSMA\uff08\u7c89\u7ea2\u8272\uff09\u7ec4\u6210\u7684\u758f\u6c34\u6027\u5d4c\u6bb5\u7ec4\u88c5\u5f62\u6210\u7684\u5d4c\u6bb5\u5171\u805a\u7269\u7684\u6a21\u62df\u5f62\u8c8c\u7684\u56fe\u50cf\uff0cSMA\u5728\u758f\u6eb6\u5242\u5d4c\u6bb5\u4e2d\u7684\u6d53\u5ea6CS\u60c5\u51b5\u5982\u4e0b\uff1a0\uff08\u9876\u90e8\uff09\uff0c0.5\uff08\u4e2d\u95f4\uff09, 1.0\uff08\u5e95\u90e8\uff09\u3002\u56fe\u4e2d\u6ca1\u6709\u663e\u793a\u6eb6\u5242\uff1b<\/p>\n

\uff08b\uff09\u805a\u5408\u7269\u56ca\u6ce1\u7684\u5e73\u5747\u534a\u5f84R\u4e0eCS\u7684\u51fd\u6570\u5173\u7cfb\uff1b<\/p>\n

\uff08c\uff09\u5355\u4e2a\u758f\u6eb6\u5242\u5d4c\u6bb5\u4f53\u79ef\u7684\u5e73\u5747\u503cV\uff0c\u4eb2\u6eb6\u5242\u5d4c\u6bb5\u94fe\u6bb5\u7684\u6709\u6548\u9762\u79efah\uff0c\u5b8c\u5168\u4f38\u5c55\u7684\u758f\u6eb6\u5242\u94fe\u6bb5\u7684\u957f\u5ea6lc\u4e0eCS\u7684\u51fd\u6570\u5173\u7cfb\uff1b<\/p>\n

\uff08d\uff09\u5806\u79ef\u53c2\u6570P\u4e0eCS\u7684\u51fd\u6570\u5173\u7cfb\u3002<\/p>\n

\u56fe5\uff1a\u4ee5PDMA\u4e3a\u5927\u5206\u5b50\u94fe\u8f6c\u79fb\u5242\uff0c\u5728\u4e59\u9187\u4e2dRAFT\u5206\u6563\u5171\u805aBzMA\u548cFMA\u7684\u793a\u610f\u56fe\u3002<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

\u56fe6\uff1aPDMA-b-P(BzMA-co-FMA)-42k-x(x = 0, 10, 20, 25, 30)\u56ca\u6ce1\u7684TEM\u548cDLS\u8868\u5f81\u7ed3\u679c\u3002<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

\uff08a-e\uff09PDMA-b-P(BzMA-co-FMA)-42k-x\u56ca\u6ce1\u7684TEM\u56fe\u50cf\uff1a\uff08a\uff09x = 0\uff0c\uff08b\uff09x = 10\uff0c\uff08c\uff09x = 20\uff0c\uff08d\uff09x = 25\uff0c\uff08e\uff09x = 30\uff1b<\/p>\n

\uff08f\uff09PDMA-b-P(BzMA-co-FMA)-42k-x\u56ca\u6ce1\u5c3a\u5bf8\u7edf\u8ba1\u5bf9FMA\u8d28\u91cf\u5206\u6570\u7684\u51fd\u6570\u5173\u7cfb\uff1b<\/p>\n

\uff08g\uff09PDMA-b-P(BzMA-co-FMA)-42k-x\u56ca\u6ce1\u7684DLS\u66f2\u7ebf\uff1b<\/p>\n

\uff08h\uff09PDMA-b-P(BzMA-co-FMA)-42k-x\u56ca\u6ce1\u7684\u6570\u5747\u6c34\u5408\u76f4\u5f84\u5bf9FMA\u8d28\u91cf\u5206\u6570\u7684\u51fd\u6570\u5173\u7cfb\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

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\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Controlling Vesicular Size via Topological Engineering of Amphiphilic Polymer in Polymerization-Induced Self-Assembly<\/a>
\n \uff08Macromolecules, 2017, DOI: 10.1021\/acs.macromol.7b02039\uff09<\/p>\n

BzMA\u4e0eFMA\u7684RAFT\u5206\u6563\u5171\u805a\u8c03\u63a7\u56ca\u6ce1\u5c3a\u5bf8\u53ca\u7ec4\u88c5\u4f53\u5f62\u8c8c\u7684\u8be6\u7ec6\u7814\u7a76\u89c1\uff1aTopological Engineering of the Amphiphilic Copolymers via RAFT Dispersion Copolymerization of Benzyl Methacrylate and 2-(Perfluorooctyl)ethyl Methacrylate for Polymeric Assemblies with Tunable Nanostructures<\/a>
\n \uff08Polymer Chemistry, 2018, DOI: 10.1039\/C8PY00029H\uff09<\/p>\n

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