{"id":116155,"date":"2017-12-11T14:00:21","date_gmt":"2017-12-11T06:00:21","guid":{"rendered":"\/\/m.iemloyee.com\/?p=116155"},"modified":"2017-12-11T09:19:00","modified_gmt":"2017-12-11T01:19:00","slug":"%e9%9d%92%e5%b2%9b%e5%82%a8%e8%83%bd%e9%99%a2energ-environ-sci-%ef%bc%9a%e9%95%81%e7%a1%ab%e7%94%b5%e6%b1%a0%e4%b8%ad%e4%b8%80%e7%a7%8d%e5%85%b7%e6%9c%89%e9%9d%9e%e4%ba%b2%e6%a0%b8%e7%89%b9%e6%80%a7","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=116155","title":{"rendered":"\u9752\u5c9b\u50a8\u80fd\u9662Energ. Environ. Sci.\uff1a\u9541\u786b\u7535\u6c60\u4e2d\u4e00\u79cd\u5177\u6709\u975e\u4eb2\u6838\u7279\u6027\u7684\u9ad8\u6548\u6709\u673a\u787c\u9178\u9541\u57fa\u7535\u89e3\u8d28"},"content":{"rendered":"

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\u8be5\u8bfe\u9898\u7ec4\u7814\u7a76\u4eba\u5458\u5229\u7528[B(HFP)3<\/sub>], MgCl2<\/sub>\u548cMg\u7c89\u672b\u57281,2-\u4e8c\u7532\u6c27\u57fa\u4e59\u70f7\u4e2d\u901a\u8fc7\u539f\u4f4d\u53cd\u5e94\u5236\u5907\u5f97\u5230\u4e86\u4ee5[B(HFP)4<\/sub>]–<\/sup>\u4e3a\u9634\u79bb\u5b50\uff0c[Mg4<\/sub>Cl6<\/sub>(DME)6<\/sub>]2+<\/sup>\u4e3a\u9633\u79bb\u5b50\u7684\u787c\u9178\u9541\u57fa\u7535\u89e3\u8d28\u3002\u5e76\u91c7\u7528\u4e86\u6838\u78c1\u5171\u632f\u3001\u8d28\u8c31\u4ee5\u53ca\u5355\u6676XRD\u65b9\u6cd5\u5bf9\u4e0a\u8ff0\u6eb6\u6db2\u8fdb\u884c\u4e86\u8868\u5f81\u3002\u8fd9\u79cd\u9541\u79bb\u5b50\u7535\u89e3\u8d28\u8868\u73b0\u51fa\u524d\u6240\u672a\u6709\u7684Mg\u7535\u9540\u548c\u5265\u843d\u6027\u80fd\uff1a\u9ad8\u8fbe3.3V\u7684\u8d1f\u6781\u7a33\u5b9a\u6027\uff08Mg\/Mg2+<\/sup>\uff09\u3001\u9ad8\u8fbe5.58 mS \/cm\u7684\u79bb\u5b50\u4f20\u8f93\u901f\u7387\u3001\u7535\u9540\u8fc7\u7a0b\u4e2d\u4ec5\u4e3a0.11V\u7684\u8fc7\u7535\u538b\u3001\u8d85\u8fc798%\u7684\u5e93\u4f26\u6548\u7387\u3002\u7531\u4e8e\u8fd9\u79cd\u7535\u89e3\u8d28\u975e\u4eb2\u6838\u673a\u7406\u7684\u5b58\u5728\uff0c\u8fd9\u79cd\u5b8c\u5168\u53ef\u9006\u7684Mg\/S\u7535\u6c60\u5177\u6709\u6781\u4f4e\u7684\u8fc7\u7535\u538b\uff0c\u4ec5\u4e3a0.3V\uff1b\u4e14\u9ad8\u8fbe1247 mAh\/g\u7684\u653e\u7535\u5bb9\u91cf\uff1b\u53d6\u5f97\u4e86\u5927\u7ea6\u4e3a1200 W\u00b7h\/kg\uff08\u9ad8\u4e8e\u8c22\u592b\u5c14\u57fa\u51c6\u768410\u500d\uff09\u7684\u6bd4\u80fd\u3002<\/p>\n

\u540c\u65f6\uff0c\u4ee5\u65b0\u578b\u787c\u9178\u9541\u57fa\u7535\u89e3\u8d28\uff0c\u9009\u53d6\u4e86\u786b\u7684\u8d28\u91cf\u5206\u6570\u4e3a80%\uff0c\u786b\u8d1f\u8377\u4e3a1.5mg\/cm2<\/sup>\u7684\u786b-\u78b3\u7eb3\u7c73\u7ba1\u4e3a\u8d1f\u6781\uff0c\u8be5\u7814\u7a76\u4eba\u5458\u6784\u5efa\u4e86\u9541\/\u786b\u7535\u6c60\uff0c\u5e76\u63a2\u7d22\u4e86\u8fd9\u4e00\u7535\u6c60\u7684\u76f8\u5173\u6027\u80fd\u3002 \u7531\u4e8e\u787c\u9178\u9541\u57fa\u7535\u89e3\u8d28\u4e0e\u786b\u57fa\u8d1f\u6781\u7684\u5b8c\u7f8e\u76f8\u5bb9\u6027\uff0c\u53ef\u4ee5\u4f7f\u9541\/\u786b\u7535\u6c60\u5b9e\u73b0\u9ad8\u7684\u80fd\u91cf\u5bc6\u5ea6\uff0c\u4e14\u5728100\u6b21\u5145\u653e\u7535\u5faa\u73af\u4e2d\u80fd\u591f\u8fbe\u5230\u9ad8\u4e8e1000 mAh\/g\u7684\u7a33\u5b9a\u7684\u653e\u7535\u5bb9\u91cf\u3002<\/p>\n

\u787c\u9178\u9541\u57fa\u7535\u89e3\u8d28\u4e0e\u57fa\u4e8e\u683c\u6797\u7eb3\u5c14\u5316\u5b66\u7684\u7535\u89e3\u8d28\u76f8\u6bd4\u5177\u6709\u5f88\u5927\u63d0\u9ad8\uff0c\u4e14\u4e0e\u57fa\u4e8eHMDS\u548c\u57fa\u4e8e\u5355\u78b3\u787c\u70f7\u7684\u9541\u7535\u89e3\u8d28\u76f8\u6bd4\uff0c\u7b80\u5355\u7684\u5408\u6210\u65b9\u6cd5\u548c\u4f18\u5f02\u7684\u7535\u6c60\u6027\u80fd\u4e5f\u662f\u787c\u9178\u9541\u57fa\u7535\u89e3\u8d28\u5f88\u5927\u7684\u4f18\u52bf\u3002\u8fd9\u4e00\u7814\u7a76\u6210\u679c\u53ef\u4ee5\u6709\u6548\u5730\u4fc3\u8fdb\u9ad8\u80fd\u91cf\u5bc6\u5ea6Mg\/S\u7535\u6c60\u7684\u7814\u53d1\uff0c\u5e76\u53ef\u4ee5\u4f5c\u4e3a\u5c06Mg\/S\u7535\u6c60\u63a8\u5411\u5e94\u7528\u81f3\u5173\u91cd\u8981\u7684\u4e00\u6b65\u3002<\/p>\n

\u3010\u56fe\u6587\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u56fe<\/strong>1<\/strong>\uff1a<\/strong>[Mg4<\/sub>Cl6<\/sub>(DME)6<\/sup>] [B(HFP)4<\/sub>]<\/strong>\u6676\u4f53\u7684\u5206\u5b50\u7ed3\u6784\u692d\u7403\u56fe\uff08\u6c22\u952e\u88ab\u5ffd\u7565\uff09<\/strong><\/p>\n

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a)Cu<\/strong>\u7535\u6781\u5728<\/strong>0.5M<\/strong>\u7684\u787c\u9178\u9541\u57fa\u7535\u89e3\u8d28\u4e2d\uff0c\u4ee5<\/strong>10mV\/s<\/strong>\u626b\u63cf\u901f\u7387\uff0c\u5728<\/strong>-0.8V<\/strong>\u4e0e<\/strong>1.8V<\/strong>\u4e4b\u95f4\u626b\u63cf\u5f97\u5230\u7684\u5faa\u73af\u4f0f\u5b89\u66f2\u7ebf\uff0c<\/strong>300<\/strong>\u6b21\u5145\u653e\u7535\u8fc7\u7a0b\uff1b<\/strong>b)<\/strong>\u6bcf\u6b21\u5145\u653e\u7535\u5faa\u73af\u4e2d\u76f8\u5e94\u7684\u7535\u9540<\/strong>\/<\/strong>\u5265\u843d\u8fc7\u7a0b\u5e93\u4f26\u6548\u7387\u66f2\u7ebf\u3002<\/strong><\/p>\n

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\u56fe<\/strong>4<\/strong>\uff1a\u787c\u9178\u9541\u57fa\u7535\u89e3\u8d28<\/strong>Mg\/Mg<\/strong>\u5bf9\u79f0\u7535\u6c60\u7684\u6781\u5316\u6027\u80fd\u53ca\u5faa\u73af\u884c\u4e3a<\/strong><\/p>\n

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a)<\/strong>0.5M<\/strong>\u7684\u787c\u9178\u9541\u57fa\u7535\u89e3\u8d28<\/strong>Mg\/Mg<\/strong>\u5bf9\u79f0\u7535\u6c60\u7684\u6781\u5316\u6027\u80fd\uff08\u7535\u6d41\u5bc6\u5ea6\u4e3a\uff1a<\/strong>0.1<\/strong>\uff0c<\/strong>0.2,0.4,0.5<\/strong>\u548c<\/strong>1mA\/cm2<\/sup><\/strong>\uff09\uff1b<\/strong>b)<\/strong>0.5M<\/strong>\u7684\u787c\u9178\u9541\u57fa\u7535\u89e3\u8d28<\/strong>Mg\/Mg<\/strong>\u5bf9\u79f0\u7535\u6c60\u957f\u65f6\u95f4\u7684\u5faa\u73af\u884c\u4e3a\uff08\u7535\u6d41\u5bc6\u5ea6\u4e3a\uff1a<\/strong>0.1mA\/cm2<\/sup><\/strong>\uff09\u5185\u5d4c\u56fe\u4e3a<\/strong>690<\/strong>\u5c0f\u65f6\u81f3<\/strong>700<\/strong>\u5c0f\u65f6\u4e4b\u95f4\u7684\u7535\u52bf\u66f2\u7ebf\u3002\u6bcf\u6b21\u5faa\u73af\u65f6\u95f4\u4e3a<\/strong>1<\/strong>\u5c0f\u65f6\uff08<\/strong>30<\/strong>\u5206\u949f\u5145\u7535\u4e0e<\/strong>30<\/strong>\u5206\u949f\u653e\u7535\uff09\u3002<\/strong><\/p>\n

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a)<\/strong>\u7c89\u672b<\/strong>XRD<\/strong>\u7ed3\u679c\uff1b<\/strong>b<\/strong>\uff09\u9541\u6c89\u79ef\u7269\u7684\u80fd\u8c31\u5206\u6790\uff1b<\/strong>c)<\/strong>\u548c<\/strong>d) <\/strong>\u4e0d\u540c\u653e\u5927\u500d\u7387\u4e0b\u9541\u6c89\u79ef\u7269\u7684<\/strong>SEM<\/strong>\u56fe\u50cf\u3002<\/strong><\/p>\n

\u56fe<\/strong>6<\/strong>\uff1a<\/strong>0.5M<\/strong>\u7684\u787c\u9178\u9541\u57fa\u7535\u89e3\u8d28\uff0c<\/strong>Mo6 <\/sub>\/S8<\/sub><\/strong>\u7535\u6c60\u7684\u7535\u5316\u5b66\u7279\u6027<\/strong><\/p>\n

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\u00a0a)<\/strong>\u524d\u4e09\u6b21\u7684<\/strong>CV<\/strong>\u66f2\u7ebf\uff1b<\/strong>b)<\/strong>\u4e0d\u540c\u7684\u5145\u7535<\/strong>–<\/strong>\u653e\u7535\u5145\u7535\u7387\u4e0b\u7684\u6bd4\u5bb9\uff1b<\/strong>c)<\/strong>\u4e0d\u540c\u5145\u7535\u7387\u4e0b\u7684\u6052\u6d41\u5145\u653e\u7535\u66f2\u7ebf\uff1b<\/strong>d)2C<\/strong>\u4e0b\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u548c\u76f8\u5e94\u7684\u5e93\u4f26\u6548\u7387\u3002<\/strong><\/p>\n

\u56fe<\/strong>7<\/strong>\uff1a\u787c\u9178\u9541\u57fa\u7535\u89e3\u8d28\u7535\u6c60\u6027\u80fd\u8fdb\u4e00\u6b65\u5206\u6790<\/strong><\/p>\n

\"\"<\/p>\n

a) <\/strong>5M<\/strong>\u7684\u787c\u9178\u9541\u57fa\u7535\u89e3\u8d28\u4e2d\uff0c\u4f5c\u4e3a\u5faa\u73af\u6b21\u6570\u51fd\u6570\u7684\u4e0d\u540c<\/strong>S-C<\/strong>\u590d\u5408\u8d1f\u6781\u7684\u653e\u7535\u5bb9\u91cf\u548c\u5e93\u4f26\u6548\u7387\u66f2\u7ebf\uff08\u653e\u7535\u901f\u7387\u4e3a\uff1a<\/strong>160mA\/g<\/strong>\uff09\uff1b<\/strong>b)-f):<\/strong>0.5M<\/strong>\u7684\u787c\u9178\u9541\u57fa\u7535\u89e3\u8d28\u4e2d<\/strong>Mg\/S-CNT<\/strong>\u7535\u6c60\u7684\u7535\u5316\u5b66\u6027\u80fd\uff1a<\/strong>b)CV<\/strong>\u66f2\u7ebf\uff1b<\/strong>c)<\/strong>\u4e0d\u540c\u5faa\u73af\u6b21\u6570\u7684\u6052\u6d41\u5145\u653e\u7535\u66f2\u7ebf\uff08\u653e\u7535\u901f\u7387\u4e3a\uff1a<\/strong>160mA\/g<\/strong>\uff09\uff1b<\/strong> d)<\/strong>\u4e0d\u540c\u5145\u653e\u7535\u7535\u6d41\u901f\u7387\u4e0b\u7684\u653e\u7535\u5bb9\u91cf\u548c\u5e93\u4f26\u6548\u7387\u66f2\u7ebf\uff1b<\/strong>e)<\/strong>\u4e0d\u540c\u5145\u653e\u7535\u7535\u6d41\u901f\u7387\u4e0b\u7684\u6052\u6d41\u5145\u653e\u7535\u66f2\u7ebf\uff1b<\/strong>f)<\/strong>\u4e0d\u540c\u5faa\u73af\u6b21\u6570\u4e0b<\/strong>EIS<\/strong>\u6d4b\u91cf\u7ed3\u679c\uff08\u5145\u653e\u7535\u901f\u7387\u4e3a\uff1a<\/strong>160mA\/g<\/strong>\uff09<\/strong> \u6709\u8272\u70b9\u4ee3\u8868\u6d4b\u8bd5\u7ed3\u679c\uff0c\u6709\u8272\u7ebf\u4e3a\u76f8\u5e94\u7684\u62df\u5408\u66f2\u7ebf\u3002<\/strong><\/p>\n

\u56fe<\/strong>8<\/strong>\uff1a<\/strong>SEM<\/strong>\u5f62\u8c8c\u53ca\u5143\u7d20\u5206\u6790<\/strong><\/p>\n

\"\"<\/p>\n

a)<\/strong>\u4e3a\u672a\u53cd\u5e94\u7684<\/strong>Mg<\/strong>\u6b63\u6781\uff1b<\/strong>b)<\/strong>\u4ee5<\/strong>2V<\/strong>\u6761\u4ef6\u4e0b<\/strong>100<\/strong>\u6b21\u5faa\u73af\u540e\u8fbe\u5230\u51e0\u4e4e\u5b8c\u5168\u5145\u7535\u72b6\u6001\u7684<\/strong>Mg<\/strong>\u6b63\u6781\uff1b<\/strong>c)<\/strong>\u56fe<\/strong>b)<\/strong>\u533a\u57df\u7684\u786b\u5143\u7d20\u5206\u5e03\u56fe\uff1b<\/strong>d)<\/strong>\u672a\u53cd\u5e94\u7684<\/strong>S-CNT<\/strong>\u8d1f\u6781\u56fe\u50cf\uff08<\/strong>d<\/strong>\uff09\u4e0e\u4ee5<\/strong>2V<\/strong>\u6761\u4ef6\u4e0b<\/strong>100<\/strong>\u6b21\u5faa\u73af\u540e\u8fbe\u5230\u51e0\u4e4e\u5b8c\u5168\u5145\u7535\u72b6\u6001\u7684<\/strong>S-CNT<\/strong>\u8d1f\u6781\u56fe\u50cf\uff08<\/strong>e<\/strong>\uff09\uff1b<\/strong>f)e<\/strong>\u533a\u57df\u7684\u9541\u5143\u7d20\u5206\u5e03\u56fe\u3002<\/strong><\/p>\n

\u8868<\/strong>1<\/strong>\uff1a\u5df2\u62a5\u9053\u4e2d<\/strong>Mg\/S<\/strong>\u7535\u6c60\u4e0d\u540c\u7535\u6781\u7684\u7535\u5316\u5b66\u6027\u80fd\u5bf9\u6bd4<\/strong><\/p>\n

\"\"<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

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\u6587\u732e\u94fe\u63a5<\/strong> \uff1aAn efficient organic magnesium borate-based electrolyte with non-nucleophilic characteristics for magnesium\u2013sulfur battery<\/a>\uff08Energ. Environ. Sci.2017.DOI\uff1a10.1039\/c7ee02304a\uff09<\/p>\n

\u901a\u8baf\u4f5c\u8005\u7b80\u4ecb<\/strong><\/p>\n

\u5d14\u5149\u78ca\uff0c\u7537\uff0c1973\u5e74\u751f\uff0c\u535a\u58eb\uff0c\u7814\u7a76\u5458\uff0c\u535a\u58eb\u751f\u5bfc\u5e08\uff0c2005\u5e74\u4e8e\u4e2d\u56fd\u79d1\u5b66\u9662\u5316\u5b66\u6240\u83b7\u5f97\u6709\u673a\u5316\u5b66\u535a\u58eb\u5b66\u4f4d\uff0c2005\u5e749\u6708\u81f32009\u5e742\u6708\u5148\u540e\u5728\u5fb7\u56fd\u9a6c\u666e\u534f\u4f1a\u9ad8\u5206\u5b50\u6240\u548c\u56fa\u6001\u6240\u4ece\u4e8b\u535a\u58eb\u540e\u7814\u7a76\u30022009\u5e742\u6708\u8d77\u4e8e\u4e2d\u79d1\u9662\u9752\u5c9b\u751f\u7269\u80fd\u6e90\u4e0e\u8fc7\u7a0b\u6240\u5de5\u4f5c\u3002<\/p>\n

2009\u5e74\u5165\u9009\u4e2d\u56fd\u79d1\u5b66\u9662\u201c\u767e\u4eba\u8ba1\u5212\u201d\uff08\u7ec8\u671f\u8bc4\u4f30\u4f18\u79c0\uff09\uff0c2009\u5e74\u83b7\u5c71\u4e1c\u7701\u81ea\u7136\u79d1\u5b66\u6770\u51fa\u9752\u5e74\u57fa\u91d1\u8d44\u52a9\uff0c2015\u5e74\u5165\u9009\u5c71\u4e1c\u7701\u201c\u6cf0\u5c71\u5b66\u8005\u7279\u8058\u4e13\u5bb6\u201d\uff0c2016\u5e74\u83b7\u56fd\u5bb6\u81ea\u7136\u79d1\u5b66\u6770\u51fa\u9752\u5e74\u57fa\u91d1\u8d44\u52a9\u3002<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u7f16\u8f91\u90e8\u65b0\u4eba\u7ec4\u666f\u5efa\u534e\u7f16\u8bd1\uff0c \u9ec4\u8d85\u5ba1\u6838\uff0c\u70b9\u6211\u52a0\u5165\u6750\u6599\u4eba\u7f16\u8f91\u90e8<\/a>\u3002<\/p>\n

\u6750\u6599\u6d4b\u8bd5\uff0c\u6570\u636e\u5206\u6790\uff0c\u4e0a<\/strong>\u6d4b\u8bd5\u8c37<\/strong><\/a>\uff01<\/strong><\/p>\n","protected":false},"excerpt":{"rendered":"

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