{"id":111312,"date":"2017-11-16T06:30:29","date_gmt":"2017-11-15T22:30:29","guid":{"rendered":"\/\/m.iemloyee.com\/?p=111312"},"modified":"2017-11-14T19:39:06","modified_gmt":"2017-11-14T11:39:06","slug":"%e5%8c%97%e4%ba%ac%e5%a4%a7%e5%ad%a6%e6%96%b0%e6%9d%90%e6%96%99%e5%ad%a6%e9%99%a2%ef%bc%9a%e5%8f%91%e7%8e%b0%e8%87%aa%e6%97%8b%e7%94%b5%e5%ad%90%e8%b6%85%e4%ba%a4%e6%8d%a2%e7%9b%b8%e4%ba%92%e4%bd%9c","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=111312","title":{"rendered":"\u5317\u4eac\u5927\u5b66\u65b0\u6750\u6599\u5b66\u9662\uff1a\u53d1\u73b0\u81ea\u65cb\u7535\u5b50\u8d85\u4ea4\u6362\u76f8\u4e92\u4f5c\u7528\u5982\u4f55\u8c03\u63a7\u9502\u7535\u6c60\u6b63\u6781\u6750\u6599"},"content":{"rendered":"<p><strong>\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n<p>\u5317\u4eac\u5927\u5b66\u6df1\u5733\u7814\u7a76\u751f\u9662\u65b0\u6750\u6599\u5b66\u9662\u6f58\u950b\u6559\u6388\u56e2\u961f\u901a\u8fc7\u7b2c\u4e00\u6027\u539f\u7406\u8ba1\u7b97\uff0c\u53d1\u73b0\u4e09\u5143\u5c42\u72b6\u6b63\u6781\u6750\u6599\u4e2d\u8fc7\u6e21\u91d1\u5c5e\u79bb\u5b50\u4e4b\u95f4\u201c\u81ea\u65cb\u7535\u5b50\u8d85\u4ea4\u6362\u201d\u4f5c\u7528\u3002\u672c\u5de5\u4f5c\u7531\u65b0\u6750\u6599\u5b66\u9662\u6f58\u950b\u6559\u6388\u3001\u90d1\u5bb6\u65b0\u526f\u7814\u7a76\u5458\u6307\u5bfc\u7855\u58eb\u751f\u6ed5\u9ad8\u70fd\u3001\u8f9b\u6f6e\u535a\u58eb\u540e\u3001\u535a\u58eb\u751f\u5353\u589e\u5e86\u5171\u540c\u5b8c\u6210\uff0c\u7814\u7a76\u6210\u679c\u4ee5\u201cRole of Superexchange Interaction on Tuning of Ni\/Li Disordering in Layered Li(Ni<sub>x<\/sub>Mn<sub>y<\/sub>Co<sub>z<\/sub>)O<sub>2<\/sub>\u201d\u4e3a\u9898\u53d1\u8868J. Phys. Chem. Lett.\u4e0a\u3002\u5728\u7f8e\u56fd\u4f2f\u514b\u5229\u56fd\u5bb6\u5b9e\u9a8c\u5ba4\u6768\u4e07\u91cc\u6559\u6388\u53c2\u4e0e\u8f6fX\u5c04\u7ebf\u7684\u5b9e\u9a8c\u6d4b\u91cf\u548c\u673a\u7406\u8ba8\u8bba\u3002\u4ee5\u4e0a\u5de5\u4f5c\u5f97\u5230\u4e86\u56fd\u5bb6\u6750\u6599\u57fa\u56e0\u7ec4\u91cd\u5927\u4e13\u9879(2016YFB0700600)\u3001\u56fd\u5bb6\u81ea\u7136\u79d1\u5b66\u57fa\u91d1(Nos. 21603007 and 51672012)\u3001\u6df1\u5733\u5e02\u79d1\u6280\u521b\u65b0\u59d4 (Nos.JCYJ20150729111733470 and JCYJ20151015162256516)\u7684\u8d44\u52a9\u652f\u6301\u3002<\/p>\n<p><strong>\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n<p><strong>\u56fe<\/strong><strong>1\u00a0\u9502\u7535\u6c60\u4e09\u5143\u5c42\u72b6\u6b63\u6781\u6750\u6599\u7ed3\u6784<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-111313 size-full\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/11\/3-30.jpg\" alt=\"\" width=\"600\" height=\"307\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/11\/3-30.jpg 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/11\/3-30-300x154.jpg 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>\uff08a\uff09\u9502\u7535\u6c60\u4e09\u5143\u5c42\u72b6\u6b63\u6781\u6750\u6599\u7ed3\u6784\uff1b<\/p>\n<p>\uff08b\uff09Ni\/Li\u53cd\u4f4d(TM)<sub>6<\/sub>\u2212O<sub>3<\/sub>\u2212Ni\u2212O<sub>3<\/sub>\u2212Li(TM)<sub>5<\/sub>\u7ed3\u6784\u57fa\u5143;<\/p>\n<p>\uff08c\uff09\u8fc7\u6e21\u91d1\u5c5e\u5c42\u4e2d\u53cd\u4f4dLi\u7684\u79bb\u5b50\u73af\u5883\u3002<\/p>\n<p><strong>\u56fe<\/strong><strong>2\u00a0\u4e09\u5143\u5c42\u72b6\u6750\u6599Ni\/Li\u53cd\u4f4d\u540e\u5f62\u6210180<sup>\u00b0<\/sup>\u8d85\u4ea4\u6362\u76f8\u4e92\u4f5c\u7528<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-111314 size-full\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/11\/4-27.jpg\" alt=\"\" width=\"600\" height=\"491\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/11\/4-27.jpg 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/11\/4-27-300x246.jpg 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p><strong>\u3010\u7814\u7a76\u5185\u5bb9\u3011<\/strong><\/p>\n<p>\u9502\u79bb\u5b50\u7535\u6c60\u4f5c\u4e3a\u6e05\u6d01\u80fd\u6e90\uff0c\u88ab\u5e7f\u6cdb\u5e94\u7528\u4e8e\u65e5\u5e38\u7535\u5b50\u4ea7\u54c1\u3001\u4eba\u5de5\u667a\u80fd\u3001\u7535\u52a8\u6c7d\u8f66\u3001\u65e0\u4eba\u673a\u7b49\u524d\u6cbf\u79d1\u6280\u9886\u57df\u3002\u6b63\u6781\u6750\u6599\u662f\u9502\u79bb\u5b50\u7535\u6c60\u7684\u6838\u5fc3\u90e8\u5206\uff0c\u76f4\u63a5\u51b3\u5b9a\u4e86\u9502\u7535\u6c60\u7684\u80fd\u91cf\u5bc6\u5ea6\u3001\u5145\u653e\u7535\u5faa\u73af\u6027\u80fd\u3001\u5b89\u5168\u6027\u3001\u6210\u672c\u7b49\u3002\u76ee\u524d\u53c2\u4e0e\u610f\u4e49\u7684\u6b63\u6781\u6750\u6599\u6709\u78f7\u9178\u94c1\u9502\uff08LiFePO<sub>4<\/sub>\uff09\u548c\u4e09\u5143\u5c42\u72b6\u6750\u6599(Li(Ni<sub>x<\/sub>Mn<sub>y<\/sub>Co<sub>z<\/sub>)O<sub>2<\/sub>)\uff0c\u5176\u4e2d\u4e09\u5143\u5c42\u72b6\u6750\u6599\u5177\u6709\u8f83\u9ad8\u7684\u80fd\u91cf\u5bc6\u5ea6\uff0c\u662f\u76ee\u524d\u9502\u79bb\u5b50\u7535\u6c60\u5e7f\u6cdb\u5e94\u7528\u7684\u6b63\u6781\u6750\u6599\uff08\u5982\u7279\u65af\u62c9\u7535\u52a8\u6c7d\u8f66\u6240\u91c7\u7528\u7684\u6b63\u6781\u6750\u6599\uff09\uff0c\u4e5f\u662f\u9502\u79bb\u5b50\u7535\u6c60\u9886\u57df\u7814\u7a76\u4e86\u51e0\u5341\u5e74\u3001\u7814\u7a76\u6700\u4e3a\u5e7f\u6cdb\u7684\u4e00\u7c7b\u6750\u6599\u3002\u5bf9\u8fd9\u7c7b\u6750\u6599\u8fdb\u884c\u7ed3\u6784\u4e0e\u6027\u80fd\u76f8\u5173\u6027\u7684\u6df1\u5165\u7814\u7a76\uff0c\u4e0d\u4ec5\u5bf9\u4ea7\u4e1a\u5e94\u7528\u6709\u91cd\u8981\u610f\u4e49\uff0c\u4e5f\u4e3a\u63a2\u7d22\u53d1\u73b0\u66f4\u597d\u7684\u6b63\u6781\u6750\u6599\u5960\u5b9a\u57fa\u7840\u3002<\/p>\n<p>\u5728\u8fd9\u7c7b\u5c42\u72b6\u6750\u6599\u4e2d\uff0c\u8fc7\u6e21\u91d1\u5c5e\u79bb\u5b50\u5c42\u4e0e\u9502\u5c42\u4ea4\u66ff\u6392\u5217\uff0c\u4e4b\u95f4\u901a\u8fc7\u6c27\u5c42\u95f4\u9694\u5f00\u3002\u7814\u7a76\u53d1\u73b0Ni\/Li\u53cd\u4f4d\u5f88\u5bb9\u6613\u53d1\u751f\u5728\u4e09\u5143\u5c42\u72b6\u6750\u6599\u4e2d\uff08\u89c1\u56fe1\uff09\uff0c\u5bf9\u5176\u6027\u80fd\u53d1\u6325\u4ea7\u751f\u5f71\u54cd\uff0c\u5982\u5f71\u54cd\u9502\u79bb\u5b50\u7684\u6269\u6563\u901f\u5ea6\u3001\u5bb9\u91cf\u53d1\u6325\u548c\u5f15\u53d1\u7ed3\u6784\u76f8\u53d8\u7b49\uff0c\u4e5f\u6709\u5c11\u6570\u62a5\u9053\u6307\u51fa\u9002\u91cf\u7684Ni\/Li\u53cd\u4f4d\u6709\u5229\u4e8e\u7535\u5316\u5b66\u5faa\u73af\u8fc7\u7a0b\u4e2d\u7684\u7ed3\u6784\u7a33\u5b9a\u3002\u6240\u4ee5Ni\/Li\u53cd\u4f4d\u5bf9\u7535\u5316\u5b66\u6027\u80fd\u7684\u5f71\u54cd\u4ee5\u53ca\u5982\u4f55\u8c03\u63a7Ni\/Li\u53cd\u4f4d\uff0c\u6210\u4e3a\u5927\u5bb6\u666e\u904d\u5173\u5fc3\u548c\u7814\u7a76\u7684\u91cd\u8981\u8bfe\u9898\u3002\u4f20\u7edf\u89c2\u70b9\u8ba4\u4e3aNi\/Li\u53cd\u4f4d\u662f\u7531\u4e8eNi<sup>2+<\/sup>\u4e0eLi+\u5177\u6709\u76f8\u4f3c\u7684\u79bb\u5b50\u534a\u5f84\uff0cNi<sup>2+<\/sup>\u5bb9\u6613\u53cd\u4f4d\u5230Li(3b)\u7684\u4f4d\u7f6e\uff0c\u4f46\u8fd9\u5f88\u96be\u89e3\u91ca\u9ad8Ni\u5c42\u72b6\u6750\u6599\u4e2d\u542b\u6709\u8f83\u591a\u7684Ni<sup>3+<\/sup>\uff0c\u4f46Ni\/Li\u53cd\u4f4d\u5374\u66f4\u5bb9\u6613\u53d1\u751f\u3002\u56e0\u6b64\u5bf9\u5176\u80cc\u540e\u7684\u673a\u7406\u8fdb\u884c\u91cd\u65b0\u7814\u7a76\u548c\u6df1\u5165\u8ba4\u8bc6\u5177\u6709\u57fa\u7840\u7406\u8bba\u548c\u4ea7\u4e1a\u5e94\u7528\u610f\u4e49\u3002<\/p>\n<p>\u5317\u4eac\u5927\u5b66\u6df1\u5733\u7814\u7a76\u751f\u9662\u65b0\u6750\u6599\u5b66\u9662\u6f58\u950b\u6559\u6388\u56e2\u961f\u901a\u8fc7\u7b2c\u4e00\u6027\u539f\u7406\u8ba1\u7b97\uff0c\u53d1\u73b0\u4e09\u5143\u5c42\u72b6\u6b63\u6781\u6750\u6599\u4e2d\u8fc7\u6e21\u91d1\u5c5e\u79bb\u5b50\u4e4b\u95f4\u201c\u81ea\u65cb\u7535\u5b50\u8d85\u4ea4\u6362\u201d\u4f5c\u7528\uff08\u4e24\u4e2a\u8fc7\u6e21\u91d1\u5c5e\uff08TM\uff09\u7684\u81ea\u65cb\u7535\u5b50\u901a\u8fc7\u6240\u5171\u540c\u94fe\u63a5\u7684\u6c27\u539f\u5b50\uff08O\uff09\u7684\u7535\u5b50\u4f5c\u4e3a\u6865\u6881\u8fdb\u884c\u7535\u5b50\u201c\u8d85\u201d\u4ea4\u6362\u76f8\u4e92\u4f5c\u7528\uff0c\u5982\u56fe2\u6240\u793a\uff09\uff0c\u4ece\u800c\u5bf9Ni\/Li\u53cd\u4f4d\u8d77\u5230\u5173\u952e\u6027\u7684\u8c03\u5236\u4f5c\u7528\u3002Ni\/Li\u53cd\u4f4d\u540e\uff0c\u53cd\u4f4dNi<sup>2+<\/sup>\u4f1a\u53d1\u751f\u81ea\u65cb\u53cd\u8f6c\uff0c\u4e0e\u8fc7\u6e21\u91d1\u5c5e\u5c42\u7684\u8fc7\u6e21\u91d1\u5c5e\u79bb\u5b50(Ni<sup>2+<\/sup>, Ni<sup>3+<\/sup>,Mn<sup>4+<\/sup>)\u5f62\u6210180\u00b0\u7684\u8d85\u4ea4\u6362\u4f5c\u7528\u3002\u7531\u4e8e\u53cd\u4f4dNi<sup>2+<\/sup>\u76843d\u8f68\u9053\u4e0eO<sup>2-<\/sup>\u76842p\u8f68\u9053\u5f62\u6210\u8f83\u5f3a\u7684\u03c3\u952e\uff0c\u8fd9\u79cd180\u00b0\u8d85\u4ea4\u6362\u4f5c\u7528\u5927\u5927\u5f3a\u4e8e\u539f\u8fc7\u6e21\u91d1\u5c5e\u5c42\u72b6\u5185\u768490\u00b0\u8d85\u4ea4\u6362\u76f8\u4e92\u4f5c\u7528\u3002\u5728\u53cd\u4f4dNi<sup>2+<\/sup>\u4e0e\u8fc7\u6e21\u91d1\u5c5e\u5c42\u8fc7\u6e21\u91d1\u5c5e\u79bb\u5b50\u5f62\u6210\u7684180\u00b0\u8d85\u4ea4\u6362\u76f8\u4e92\u4f5c\u7528\u4e2d\uff0cNi<sup>2+<\/sup>-O<sup>2<\/sup>-Ni<sup>2+<\/sup>\u6700\u5f3a\uff0cNi<sup>2+<\/sup>-O<sup>2<\/sup>-Co<sup>3+<\/sup>\u6700\u5f31\uff0c\u6240\u4ee5Ni\/Li\u53cd\u4f4d\u6700\u6613\u53d1\u751f\u5728\u53cd\u4f4d\u540e\u80fd\u5f62\u6210\u8f83\u591a\u7ebf\u6027Ni<sup>2+<\/sup>-O<sup>2<\/sup>-Ni<sup>2+<\/sup>\u7684\u4f4d\u7f6e\u3002\u8fd9\u4e5f\u89e3\u91ca\u4e86\u4e3a\u4ec0\u4e48\u5728\u4ee5\u5f80\u7684\u5b9e\u9a8c\u62a5\u9053\u4e2d\u53d1\u73b0\u9ad8Ni\u5c24\u5176\u662f\u542b\u6709\u66f4\u591aNi<sup>2+<\/sup>\u7684\u4e09\u5143\u5c42\u72b6\u6750\u6599\u4e2d\u542b\u6709\u8f83\u591a\u7684Ni\/Li\u53cd\u4f4d\uff0c\u800c\u5728\u201cNi=Mn\u201d\u4e09\u5143\u5c42\u72b6\u6b63\u6781\u6750\u6599\u4e2d\uff0cCo\u80fd\u6291\u5236Ni\/Li\u53cd\u4f4d\u3002\u57fa\u4e8e\u8d85\u4ea4\u6362\u4f5c\u7528\u6a21\u578b\uff0c\u8bfe\u9898\u7ec4\u8fd8\u53d1\u73b0\u5728\u9ad8Ni\u542b\u6709Ni<sup>2+<\/sup>\/Ni<sup>3+<\/sup>\u6df7\u5408\u4ef7\u6001\u7684\u5c42\u72b6\u6750\u6599\u4e2d\uff0cNi<sup>3+<\/sup>\u4f1a\u4f18\u5148\u53cd\u4f4d\u5230Li\u5c42\u5f62\u6210Ni<sup>2+<\/sup>\uff0c\u53d1\u751f\u81ea\u65cb\u53cd\u8f6c\u5f62\u6210\u66f4\u591a\u7684\u7ebf\u6027Ni<sup>2+<\/sup>-O<sup>2<\/sup>-Ni<sup>2+<\/sup>\u8d85\u4ea4\u6362\u4f5c\u7528\u3002\u540c\u65f6\u7531\u4e8e\u7535\u8377\u8865\u507f\u4f5c\u7528\uff0c\u539fNi<sup>3+<\/sup>\u9644\u8fd1\u7684Co<sup>3+<\/sup>\u4f1a\u53d8\u5230Co<sup>4+<\/sup>\uff0c\u8fd9\u4e5f\u662f\u8bfe\u9898\u7ec4\u5728\u56fd\u9645\u4e0a\u9996\u6b21\u9884\u6d4b\u5728\u9ad8Ni\u4e09\u5143\u5c42\u72b6\u6750\u6599\u4e2d\u6709Co<sup>4+<\/sup>\u5b58\u5728\u3002\u8be5\u9884\u6d4b\u4e5f\u5f97\u5230\u4e86\u7f8e\u56fd\u4f2f\u514b\u5229\u56fd\u5bb6\u5b9e\u9a8c\u5ba4\u7684\u540c\u6b65\u8f90\u5c04\u8f6fX\u5c04\u7ebf\u5438\u6536\u8c31\u7684\u8bc1\u5b9e\u3002\u4e0a\u8ff0\u53d1\u73b0\u4e0d\u4ec5\u4e3a\u4e09\u5143\u5c42\u72b6\u6b63\u6781\u6750\u6599\u957f\u671f\u4ee5\u6765\u7684Ni\/Li\u53cd\u4f4d\u73b0\u8c61\u63d0\u4f9b\u4e86\u5f88\u597d\u7684\u673a\u7406\u89e3\u91ca\uff0c\u4e5f\u4e3a\u4eca\u540e\u4e09\u5143\u6b63\u6781\u6750\u6599\u7684\u53cd\u4f4d\u7f3a\u9677\u53ef\u63a7\u8c03\u5236\u3001\u65b0\u578b\u4e09\u5143\u6750\u6599\u7684\u8bbe\u8ba1\u63d0\u4f9b\u4e86\u91cd\u8981\u7ebf\u7d22\uff0c\u5982\u5bfb\u627e\u53ef\u66ff\u6362Co\u7684\u66f4\u4fbf\u5b9c\u7684\u91d1\u5c5e\u79bb\u5b50\u3002<\/p>\n<p>\u539f\u6587\u94fe\u63a5\uff1a<a href=\"http:\/\/pkunews.pku.edu.cn\/xxfz\/2017-11\/07\/content_299983.htm\" target=\"_blank\" rel=\"noopener\">http:\/\/pkunews.pku.edu.cn\/xxfz\/2017-11\/07\/content_299983.htm<\/a>\u3002<\/p>\n<p>\u6587\u732e\u94fe\u63a5\uff1a<a href=\"http:\/\/pubs.acs.org\/doi\/10.1021\/acs.jpclett.7b02498\" target=\"_blank\" rel=\"noopener\">Role of Superexchange Interaction on Tuning of Ni\/Li Disordering in Layered Li(NixMnyCoz)O2<\/a>\uff08J. Phys. Chem. 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