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1 \u4ea7\u751f\u4e0e\u53d1\u5c55<\/strong><\/span><\/p>\n

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2 \u5e94\u7528\u9886\u57df<\/strong><\/span><\/p>\n

\u6700\u8fd130\u5e74\u8d28\u8c31\u5b66\u5728\u5404\u4e2a\u65b9\u9762\u90fd\u83b7\u5f97\u4e86\u6781\u5927\u7684\u53d1\u5c55\u3002\u65b0\u7684\u79bb\u5b50\u5316\u65b9\u6cd5\u5982\u573a\u81f4\u7535\u79bb(FI)\u3001\u573a\u89e3\u5438\u7535\u79bbF(D)\u3001\u5316\u5b66\u7535\u79bb(CI)\u3001\u6fc0\u5149\u79bb\u5b50\u5316\u3001\u7b49\u79bb\u5b50\u4f53\u6cd5\u7b49\u4e0d\u65ad\u51fa\u73b0\u3002\u590d\u6742\u7684\u3001\u9ad8\u6027\u80fd\u7684\u5546\u54c1\u4eea\u5668\u4e0d\u65ad\u63a8\u51fa,\u5982\u79bb\u5b50\u63a2\u9488\u8d28\u8c31\u4eea\u3001\u78c1\u573a\u578b\u7684\u4e32\u8054\u8d28\u8c31\u4eea\u3001\u79bb\u5b50\u56de\u65cb\u5171\u632f\u4e00\u5085\u7acb\u53f6\u53d8\u6362\u8d28\u8c31\u4eea\u7b49\u3002\u6db2\u76f8\u8272\u8c31\u4e0e\u8d28\u8c31\u7684\u8054\u7528\u5728\u8fd110\u5e74\u6765\u6709\u7a81\u7834\u6027\u8fdb\u5c55,\u5df1\u8fdb\u5165\u5b9e\u7528\u9636\u6bb5\u3002\u53e6\u4e00\u65b9\u9762,\u4f4e\u4ef7\u4f4d\u3001\u7b80\u6613\u578b\u4eea\u5668\u7684\u63a8\u51fa,\u5bf9\u6269\u5927\u548c\u666e\u53ca\u8d28\u8c31\u5206\u6790\u7684\u5e94\u7528\u8d77\u4e86\u5f88\u5927\u7684\u4f5c\u7528\u3002<\/p>\n

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2.1 \u4e2d\u836f\u4ee3\u8c22\u53ca\u5176\u836f\u4ee3\u52a8\u529b\u5b66:<\/strong><\/p>\n

1980\u5e74\u4ee5\u6765 \u4e2d\u836f\u4ee3\u8c22\u53ca\u5176\u836f\u4ee3\u52a8\u529b\u5b66\u7814\u7a76\u7684\u6df1\u5ea6\u548c\u5e7f\u5ea6\u6709\u4e86\u8f83\u5927\u5e45\u5ea6\u7684\u63d0\u9ad8,\u8fd1\u5e74\u6765\u7531\u4e8e\u6db2\u76f8\u8272\u8c31\u548c\u8d28\u8c31\u8054\u7528\u6280\u672f\u7684\u8fc5\u731b\u53d1\u5c55,\u4f7f\u5f97\u76ee\u524d\u8d28\u8c31\u5c24\u5176\u662f\u4e32\u8054\u8d28\u8c31\u5df2\u6210\u4e3a\u4e2d\u836f\u4ee3\u8c22\u7269\u7814\u7a76\u548c\u68c0\u6d4b\u7684\u91cd\u8981\u5de5\u5177\u3002\u836f\u7269\u4ee3\u8c22\u7814\u7a76\u662f\u836f\u7269\u5f00\u53d1\u8fc7\u7a0b\u4e2d\u975e\u5e38\u91cd\u8981\u7684\u4e00\u6b65,\u901a\u5e38\u7684\u505a\u6cd5\u662f\u9996\u5148\u6536\u96c6\u6837\u54c1,\u7528\u6eb6\u5242\u63d0\u53d6\u6216\u67f1\u8272\u8c31\u6216\u9ad8\u538b\u6db2\u76f8\u8272\u8c31\u5236\u5907\u5f97\u5230\u7eaf\u54c1,\u518d\u8fdb\u4e00\u6b65\u5bf9\u539f\u836f\u548c\u4ee3\u8c22\u7269\u8fdb\u884c\u7d2b\u5916\u3001\u7ea2\u5916\u3001\u8d28\u8c31\u3001\u6838\u78c1\u5171\u632f\u7b49\u5149\u8c31\u5206\u6790,\u63a8\u65ad\u4ee3\u8c22\u7269\u7684\u7ed3\u6784\u3002\u6db2\u76f8\u8272\u8c31\u548c\u8d28\u8c31\u8054\u7528\u5927\u5927\u8282\u7701\u4e86\u6837\u54c1\u5904\u7406\u548c\u63d0\u53d6\u5de5\u4f5c,\u540c\u65f6\u7531\u4e8e\u91c7\u7528\u4e32\u8054\u8d28\u8c31\u68c0\u6d4b\u548c\u56fe\u8c31\u89e3\u6790\u53ef\u4ee5\u4e86\u89e3\u6bcd\u4f53\u836f\u7269\u7684\u4ee3\u8c22\u4ea7\u7269\u3002<\/p>\n

2.2 \u76d1\u6d4b\u52a0\u5de5\u98df\u54c1\u4e2d\u7684\u4e09\u805a\u6c30\u80fa\u53ca\u5176\u6c34\u89e3\u4ea7\u7269:<\/strong><\/p>\n

2007\u5e747\u6708,\u7f8e\u56fd\u56fd\u5bb6\u98df\u54c1\u5b89\u5168\u4e0e\u6280\u672f\u4e2d\u5fc3\u5f00\u59cb\u4f7f\u7528\u914d\u5907\u4e86Thermo Scientific AccelaTM\u9ad8\u901f\u6db2\u76f8\u7cfb\u7edf\u7684TSQ Quantum\u4e09\u91cd\u56db\u6781\u6746\u8d28\u8c31\u4eea, \u5efa\u7acb\u76d1\u6d4b\u52a0\u5de5\u98df\u54c1\u4e2d\u7684\u4e09\u805a\u6c30\u80fa\u53ca\u5176\u6c34\u89e3\u4ea7\u7269\u7684\u6db2\u76f8\u8272\u8c312\u4e32\u8054\u8d28\u8c31\u65b9\u6cd5\u3002TSQ Quantum\u53ef\u4ee5\u4f7f\u7528\u9ad8\u5ea6\u9009\u62e9\u53cd\u5e94\u76d1\u6d4b(H2SRM)\u6a21\u5f0f\u7684\u4eea\u5668,\u8fd9\u79cd\u6a21\u5f0f\u4f7f\u52a8\u7269\u7ec4\u7ec7\u7b49\u590d\u6742\u6837\u54c1\u7684\u5feb\u901f\u548c\u6709\u6548\u5206\u6790\u66f4\u5bb9\u6613\u3002\u8fd9\u4e2a\u65b9\u6cd5\u7528Thermo Scientific\u7684LC2MS\/MS\u5f97\u51fa\u7684\u7cbe\u5bc6\u5ea6\u548c\u51c6\u786e\u5ea6\u503c,\u5b8c\u5168\u6ee1\u8db3\u98df\u54c1\u836f\u54c1\u76d1\u7763\u7ba1\u7406\u5c40\u5173\u4e8e\u5206\u6790\u65b9\u6cd5\u5efa\u7acb\u548c\u786e\u8bc1\u7684\u6307\u5bfc\u539f\u5219\u7684\u8981\u6c42\u3002<\/p>\n

\u6d4b\u5b9a\u9cb6\u9c7c\u4e2d\u7684\u4e09\u805a\u6c30\u80fa\u6b8b\u7559\u7684\u73b0\u6709\u65b9\u6cd5(\u5b9e\u9a8c\u5ba4\u4fe1\u606f\u901a\u62a5No. 4396)\u662f\u7531\u4f4d\u4e8e\u4e39\u4f5b\u7684\u98df\u54c1\u836f\u54c1\u76d1\u7763\u7ba1\u7406\u5c40\u52a8\u7269\u836f\u7269\u7814\u7a76\u4e2d\u5fc3\u5efa\u7acb\u7684\u3002\u8be5\u65b9\u6cd5\u4f7f\u7528TSQ Quantum\u8d28\u8c31\u4eea,\u914d\u5907\u4e86Thermo Scientific\u7684SurveyorTM\u578bLC2MS\u578b\u6db2\u76f8\u6cf5\u548c\u81ea\u52a8\u8fdb\u6837\u5668\u3002<\/p>\n

\u4ece\u542b\u670910ppb\u4e09\u805a\u6c30\u80fa\u7684\u52a0\u5de5\u7684\u9cb6\u9c7c\u4e2d\u5f97\u5230\u7684\u603b\u79bb\u5b50\u8272\u8c31\u56fe,ESI\u6b63\u79bb\u5b50\u68c0\u6d4b\u3002\u63d0\u53d6\u7269\u7684\u5206\u6790\u91c7\u7528Thermo Scientific\u7684150\u00d7211mm BioBasicTMAX\u8272\u8c31\u67f1\u548cAccela\u6db2\u76f8\u7cfb\u7edf\u3002\u5206\u6790\u7269\u7684\u68c0\u6d4b\u901a\u8fc7TSQ Quantum\u5b8c\u6210,\u76d1\u6d4b\u7684\u79bb\u5b50\u5bf9\u4e3am\/z128\u219285\u548cm\/z 128\u219268\u3002\u65b9\u6cd5\u8868\u660eThermo Scientific\u7684\u4eea\u5668\u80fd\u591f\u68c0\u6d4b\u51fa\u9cb6\u9c7c\u63d0\u53d6\u7269\u4e2d10ppb\u6c34\u5e73\u7684\u4e09\u805a\u6c30\u80fa,\u8d85\u8fc7\u4e86\u98df\u54c1\u836f\u54c1\u76d1\u7763\u7ba1\u7406\u5c40\u89c4\u5b9a\u7684\u8981\u6c42\u3002<\/p>\n

2.3 \u98df\u54c1<\/strong><\/p>\n

\u4e39\u9ea6\u7f57\u65af\u57fa\u65af\u4e00\u5b9e\u9a8c\u5ba4\u53d1\u660e\u4e00\u79cd\u5e26\u6709\u8d28\u8c31\u4eea\u7684\u7a7a\u8c03\u88c5\u7f6e\u3002\u8be5\u88c5\u7f6e\u53ef\u7ed8\u5236\u4ea7\u54c1\u4e2d60\u591a\u79cd\u5143\u7d20\u7684\u76f8\u5bf9\u542b\u91cf,\u53ef\u4e0e\u519c\u4ea7\u54c1\u6837\u54c1\u7684\u8d28\u8c31\u4eea\u56fe\u8c31\u8fdb\u884c\u5bf9\u6bd4,\u4ece\u800c\u53ef\u5f97\u77e5\u8fd9\u4e9b\u519c\u4ea7\u54c1\u6709\u65e0\u5316\u80a5\u4e0e\u519c\u836f\u6b8b\u7559\u7269,\u786e\u8ba4\u662f\u5426\u662f\u4e0d\u542b\u5316\u80a5\u4e0e\u519c\u836f\u6b8b\u7559\u7269\u7684\u771f\u6b63\u7eff\u8272\u98df\u54c1,\u4ece\u800c\u53ef\u4ee5\u8bc6\u522b\u6d41\u901a\u9886\u57df\u4e2d\u5546\u8d29\u7ed9\u4f2a\u52a3\u519c\u4ea7\u54c1\u8d34\u4e0a\u201c\u7eff\u8272\u98df\u54c1\u201d\u7684\u4f2a\u52a3\u7eff\u8272\u98df\u54c1\u3002(\u6458\u81eaZGSPB,2002211225)<\/p>\n

\u56fd\u5185\u81ea\u884c\u7814\u5236\u7684\u9ad8\u5206\u8fa8\u7387ESI-TOF-MS\u5206\u6790\u4ece\u5927\u8c46\u6bdb\u6cb9\u4e2d\u8403\u53d6\u51fa\u6765\u7684\u78f7\u8102,\u5b9e\u73b0\u4e86\u56fd\u5185\u9996\u6b21\u7528\u81ea\u5236ESI-TOF-MS\u5206\u6790\u5927\u8c46\u78f7\u8102\u4e2d\u78f7\u8102\u915e\u80c6\u78b1\u3002\u7ed3\u679c\u8868\u660e,\u5229\u7528ESI-TOF-MS\u5171\u68c0\u6d4b\u51fa\u4e86\u5927\u8c46\u78f7\u8102\u4e2d\u768452\u79cd\u78f7\u8102\u915e\u80c6\u78b1\u3002<\/p>\n

2.4 \u533b\u5b66<\/strong><\/p>\n

\u8868\u9762\u52a0\u5f3a\u6fc0\u5149\u89e3\u6790\u7535\u79bb\u98de\u884c\u65f6\u95f4\u8d28\u8c31\u4eea(SELDI-TOFMS)\u662f\u4e00\u79cd\u65b0\u7684\u86cb\u767d\u8d28\u68c0\u6d4b\u6280\u672f,\u4e0e\u4f20\u7edf\u7684\u86cb\u767d\u8d28\u7ec4\u5b66\u65b9\u6cd5\u76f8\u6bd4,\u8be5\u6280\u672f\u5177\u6709\u5feb\u901f\u3001\u7075\u654f\u3001\u9ad8\u901a\u91cf\u7b49\u7279\u70b9\u3002\u8fd0\u7528\u8be5\u6280\u672f\u5236\u6210\u7684\u86cb\u767d\u8d28\u82af\u7247\u8d28\u8c31\u4eea\u5df2\u6210\u4e3a\u86cb\u767d\u8d28\u7ec4\u5b66\u7814\u7a76\u4e2d\u7684\u91cd\u8981\u5de5\u5177\u3002<\/p>\n

2.5 \u5730\u8d28<\/strong><\/p>\n

\u4f34\u968f\u73b0\u4ee3\u94bb\u4e95\u6280\u672f\u7684\u98de\u901f\u53d1\u5c55,\u6108\u52a0\u8981\u6c42\u5f55\u4e95\u516c\u53f8\u80fd\u591f\u63d0\u4f9b\u66f4\u52a0\u8fc5\u6377\u7684\u591a\u65b9\u9762\u5f55\u4e95\u8d44\u6599,\u57fa\u4e8e\u8fd9\u79cd\u60c5\u51b5,\u6cd5\u56fd\u5730\u8d28\u670d\u52a1\u516c\u53f8\u5f00\u5c55\u4e86\u80fd\u591f\u5e94\u7528\u4e8e\u73b0\u573a\u7684\u540c\u4f4d\u7d20\u8d28\u8c31\u4eea\u7684\u7814\u5236\u5de5\u4f5c\u3002\u8be5\u5957\u4eea\u5668\u7684\u7814\u5236,\u5145\u5206\u5229\u7528\u4e86\u540c\u4f4d\u7d20\u8d28\u8c31\u6280\u672f\u7684\u68c0\u6d4b\u539f\u7406,\u4e3a\u73b0\u573a\u5f55\u4e95\u70c3\u7c7b\u6c14\u4f53\u68c0\u6d4b\u589e\u52a0\u4e86\u6709\u6548\u7684\u8f85\u52a9\u624b\u6bb5\u3002\u5177\u6709\u76f8\u540c\u8d28\u5b50\u6570\u3001\u4e0d\u540c\u4e2d\u5b50\u6570\u6216\u4e0d\u540c\u8d28\u91cf\u6570\u7684\u540c\u4e00\u5316\u5b66\u5143\u7d20\u7684\u4e0d\u540c\u6838\u7d20\u4e92\u4e3a\u540c\u4f4d\u7d20,\u540c\u79cd\u5143\u7d20\u7684\u5404\u79cd\u540c\u4f4d\u7d20\u8d28\u91cf\u4e0d\u540c, \u4f46\u5316\u5b66\u6027\u8d28\u513f\u4e4e\u76f8\u540c,\u56e0\u6b64\u53ef\u4ee5\u901a\u8fc7\u6d4b\u91cf\u6c14\u4f53\u7684\u540c\u4f4d\u7d20\u5f97\u5230\u5177\u6709\u76f8\u540c\u8d28\u91cf\u5206\u6570\u7684\u70c3\u7c7b\u6c14\u4f53\u8d28\u91cf\u6d53\u5ea6\u3002<\/p>\n

2.6 \u5206\u6790\u7ec6\u5c0f\u6c14\u6eb6\u80f6\u7c92\u5b50<\/strong><\/p>\n

\u7f8e\u56fdDelaware\u5927\u5b66Johnston\u7b49\u4eba\u7814\u5236\u51fa\u7528\u4f5c\u8d85\u7ec6\u7c92\u5b50\u5206\u6790\u7684\u6fc0\u5149\u8d28\u8c31\u4eea,\u7528\u6fc0\u5149\u70e7\u707c\u6cd5\u5b9e\u65f6\u5206\u6790\u5355\u4e2a\u6c14\u6eb6\u80f6\u7c92\u5b50,\u7c92\u5b50\u76f4\u5f84\u4e3a10\uff5e150nm,\u6bd4\u73b0\u6709\u540c\u7c7b\u4eea\u5668\u80fd\u6d4b\u91cf\u7684\u7c92\u5b50\u76f4\u5f84\u5c0f\u4e00\u4e2a\u91cf\u7ea7\u3002<\/p>\n

2.7 \u94a2\u94c1\u751f\u4ea7<\/strong><\/p>\n

\u8d28\u8c31\u4eea\u5728\u94a2\u94c1\u5382\u6210\u529f\u7528\u4e8e:\u9ad8\u7089\u7089\u6c14\u5206\u6790\u3001\u8f6c\u7089\u7089\u6c14\u5206\u6790(BOS,BOF)\u3001\u7126\u7089\u7089\u6c14\u5206\u6790\u3001\u6df7\u5408\u7ad9\u6c14\u4f53\u5206\u6790\u7b49\u90e8\u95e8\u3002<\/p>\n

2.8 \u6c7d\u8f6e\u673a\u771f\u7a7a\u7cfb\u7edf\u68c0\u6f0f<\/strong><\/p>\n

\u56fd\u5185\u7ecf\u8fc7\u51e0\u5e74\u6765\u4f7f\u7528\u5fb7\u56fd\u83b1\u5b9d\u516c\u53f8\u6c26\u8d28\u8c31\u4eea\u68c0\u6f0f\u7684\u7ecf\u9a8c\u8868\u660e,\u9488\u5bf9\u673a\u7ec4\u771f\u7a7a\u7cfb\u7edf\u590d\u6742,\u7ba1\u9053\u7e41\u591a\u4e14\u88ab\u4fdd\u6e29\u96be\u4ee5\u68c0\u6d4b\u7684\u7279\u70b9,\u5728\u8fdb\u884c\u68c0\u6f0f\u524d,\u5e94\u5bf9\u673a\u7ec4\u7684\u8fd0\u884c\u60c5\u51b5\u548c\u6027\u80fd\u6307\u6807\u4f5c\u8ba4\u771f\u5206\u6790\u3002\u7ed3\u5408\u4ee5\u5f80\u5927\u3001\u5c0f\u4fee\u505c\u673a\u704c\u6c34\u8bd5\u9a8c,\u6d88\u7f3a\u60c5\u51b5\u6982\u7565\u5730\u5217\u51fa\u91cd\u70b9\u68c0\u6f0f\u90e8\u4f4d,\u4ece\u800c\u7f29\u77ed\u68c0\u6f0f\u65f6\u95f4,\u63d0\u9ad8\u67e5\u6f0f\u6548\u7387,\u6355\u6349\u91cd\u8981\u6f0f\u70b9\u3002\u5728\u5bf9\u970d\u5dde\u7535\u53821\u53f7\u30012\u53f7\u673a(100MW),\u67f3\u6797\u7535\u53821\u53f7\u673a(100MW),\u6986\u793e\u7535\u53821\u53f7\u30012\u53f7(100MW),\u795e\u5934\u7b2c\u4e00\u53d1\u7535\u53824\u53f7(200MW)\u8fdb\u884c\u7684\u68c0\u6f0f,\u5747\u53d6\u5f97\u4e86\u9884\u671f\u7684\u6548\u679c\u3002<\/p>\n

2.9 \u73af\u5883\u3001\u751f\u7269\u5206\u6790<\/strong><\/p>\n

\u4e32\u8054\u8d28\u8c31\u6280\u672f\u4f5c\u4e3a\u5206\u6790\u6df7\u5408\u7269\u548c\u5206\u5b50\u7ed3\u6784\u9274\u5b9a\u7684\u91cd\u8981\u624b\u6bb5,\u5f88\u65e9\u4ee5\u524d\u5df2\u5728\u5927\u578b\u8d28\u8c31\u4eea\u4e0a\u5f97\u5230\u5e94\u7528,\u5728\u4e24\u4e2a\u524d\u540e\u4e32\u8054\u7684\u8d28\u8c31\/\u8d28\u8c31\u4eea\u4e2d,\u524d\u7ea7\u8d28\u8c31\u4e3b\u8981\u7528\u4e8e\u62c5\u4efb\u5206\u79bb\u5de5\u4f5c,\u5728\u6837\u54c1\u88ab\u7535\u79bb\u540e,\u5b83\u53ea\u5141\u8bb8\u88ab\u5206\u6790\u7684\u76ee\u6807\u5316\u5408\u7269\u7684\u6bcd\u4ee3\u79bb\u5b50\u788e\u7247,\u7ecf\u8fc7\u78b0\u649e\u88c2\u89e3\u540e,\u7531\u7b2c\u4e8c\u7ea7\u8d28\u8c31\u5206\u6790\u88c2\u89e3\u540e\u4ea7\u751f\u7684\u79bb\u5b50\u788e\u7247,\u7531\u4e8e\u4e0a\u8ff0\u8fc7\u7a0b\u7684\u5b8c\u6210\u81f3\u5c11\u9700\u8981\u4e09\u4e2a\u8d28\u91cf\u5206\u79bb\u5668\u4e32\u8054\u800c\u6210,\u6545\u5728\u5927\u578b\u8d28\u8c31\u4eea\u4e0a\u5e94\u7528\u4e32\u8054\u8d28\u8c31\u6280\u672f\u6210\u672c\u8f83\u9ad8,\u800c\u4e14\u64cd\u4f5c\u6bd4\u8f83\u590d\u6742,\u4ece\u800c\u9650\u5236\u4e86\u8be5\u6280\u672f\u7684\u5e7f\u6cdb\u5e94\u7528\u3002\u968f\u7740\u79bb\u5b50\u9631\u8d28\u8c31\u4eea\u7684\u53d1\u5c55,\u5229\u7528\u5176\u53ef\u5b9e\u73b0\u65f6\u95f4\u4e32\u8054\u7684\u7279\u6027,\u5373\u4e32\u8054\u8d28\u8c31\u7684\u6bcf\u4e2a\u9636\u6bb5\u5728\u4e0d\u540c\u65f6\u95f4\u6bb5\u8fdb\u884c,\u4f7f\u7528\u540c\u4e00\u4e2a\u79bb\u5b50\u9631\u8d28\u91cf\u5206\u79bb\u88c5\u7f6e\u5c31\u53ef\u4ee5\u5b8c\u6210\u4e32\u8054\u8d28\u8c31\u7684\u5206\u6790,\u751a\u81f3\u53ef\u4ee5\u8fdb\u884c\u591a\u7ea7\u8d28\u8c31\u7684\u5206\u6790,Varian \u516c\u53f8\u7684Saturn\u4e32\u8054\u8d28\u8c31\u4eea\u76ee\u524d\u53ef\u4ee5\u505a\u5230MS6\u3002\u4ece\u800c\u5927\u5927\u964d\u4f4e\u4e32\u8054\u8d28\u8c31\u5206\u6790\u7684\u6210\u672c,\u800c\u4e14\u6027\u80fd\u4f18\u5f02\u7684\u5de5\u4f5c\u7ad9\u8f6f\u4ef6\u4e5f\u4f7f\u8be5\u5206\u6790\u7684\u64cd\u4f5c\u53d8\u5f97\u5341\u5206\u5bb9\u6613\u3002\u76ee\u524d,\u8be5\u6280\u672f\u5728\u73af\u5883\u5206\u6790\u3001\u98df\u54c1\u5206\u6790\u3001\u751f\u7269\u5206\u6790\u7b49\u65b9\u9762\u5f97\u5230\u4e86\u5e7f\u6cdb\u7684\u5e94\u7528\u3002\u5b83\u4e0d\u4ec5\u9002\u7528\u4e8e\u590d\u6742\u57fa\u4f53\u6df7\u5408\u7269\u7684\u5b9a\u6027\u5206\u6790,\u800c\u4e14\u53ef\u4ee5\u5229\u7528\u5f97\u5230\u4e8c\u7ea7\u8d28\u8c31\u7ed3\u679c\u8fdb\u884c\u5b9a\u91cf\u3002<\/p>\n

2.10 \u5730\u7403\u5316\u5b66<\/strong><\/p>\n

\u540c\u4f4d\u7d20\u6bd4\u7387\u8d28\u8c31\u4eea(isotoperatiomass spectrometers,IRMS)\u662f\u8fd1\u4e9b\u5e74\u53d1\u5c55\u8d77\u6765\u7684\u7528\u4e8e\u6d4b\u5b9a\u67d0\u4e9b\u7a33\u5b9a\u540c\u4f4d\u7d20\u7ec4\u6210\u7684\u4eea\u5668,\u5728\u8bf8\u591a\u9886\u57df\u4e2d\u90fd\u5c55\u73b0\u51fa\u5e7f\u9614\u7684\u5e94\u7528\u524d\u666f\u3002\u7531\u4e8e\u7a33\u5b9a\u540c\u4f4d\u7d20\u7ec4\u6210\u4e2d\u8574\u85cf\u7740\u4e30\u5bcc\u7684\u5730\u7403\u5316\u5b66\u4fe1\u606f,\u901a\u8fc7\u7814\u7a76\u5176\u7ec4\u6210\u53ef\u4ee5\u63ed\u793a\u5730\u7403\u5316\u5b66\u8fc7\u7a0b\u4e2d\u7684\u8bf8\u591a\u65b9\u9762\u7684\u4fe1\u606f\u3002\u6240\u4ee5IRMS\u6280\u672f\u548c\u540c\u4f4d\u7d20\u4e00\u8d77\u4f5c\u4e3a\u4e00\u79cd\u65b0\u7684\u6709\u6548\u624b\u6bb5\u5728\u5730\u7403\u5316\u5b66\u7814\u7a76\u4e2d\u6709\u7740\u8d8a\u6765\u8d8a\u5e7f\u6cdb\u7684\u5e94\u7528\u3002<\/p>\n

2.11 \u5730\u5b66\u3001\u8003\u53e4\u548c\u751f\u7269\u533b\u5b66<\/strong><\/p>\n

\u5728\u56fd\u5bb6\u79d1\u6280\u90e8\u3001\u4e2d\u56fd\u79d1\u5b66\u9662\u548c\u6559\u80b2\u90e8\u7684\u8054\u5408\u652f\u6301\u4e0b,\u7531\u4e2d\u56fd\u79d1\u5b66\u9662\u5730\u7403\u73af\u5883\u7814\u7a76\u6240\u4e0e\u897f\u5b89\u4ea4\u901a\u5927\u5b66\u8054\u5408\u7b79\u5efa\u7684\u897f\u5b89\u52a0\u901f\u5668\u8d28\u8c31\u4e2d\u5fc3\u7684\u4e00\u53f03MV\u7684\u591a\u6838\u7d20\u5206\u6790\u52a0\u901f\u5668\u8d28\u8c31\u4eea(Xi\u2019an-AMS)\u53ca\u5176\u6837\u54c1\u5236\u5907\u7cfb\u7edf\u4ee5\u5730\u5b66\u3001\u8003\u53e4\u548c\u751f\u7269\u533b\u5b66\u7814\u7a76\u4e3a\u4e3b,\u591a\u5b66\u79d1\u5171\u4eab,\u8fd1\u671f\u4ee510Be\u548c14C\u5206\u6790\u4e3a\u4e3b,\u4e14\u4e3a\u5c3d\u5feb\u5f00\u5c5526Al\u548c129I\u5206\u6790\u4f5c\u6280\u672f\u51c6\u5907\u3002\u6b63\u5e38\u8fd0\u884c\u60c5\u51b5\u4e0b,\u6bcf\u5e74\u5206\u67902500 \u6837\u54c1,\u73b0\u4ee3\u6837\u54c1\u768414C\u6d4b\u91cf\u7cbe\u5ea6\u4f18\u4e8e0.5%,\u53ef\u8fbe0.2\uff05-0.3\uff05,10Be\u63a2\u6d4b\u7075\u654f\u5ea6\u53ef\u8fbe10-15 \u91cf\u7ea7\u3002<\/p>\n

2.12 \u8f7d\u4eba\u822a\u5929<\/strong><\/p>\n

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GC\u2014TCD\u5931\u6548\u65f6,MS\u5355\u72ec\u6d4b\u8bd5,\u7528\u4e8e\u76d1\u6d4b\u4f18\u5148\u7ea7\u2160\u6c14\u4f53\u7684\u68c0\u6d4b\u3002\u8fd9\u79cd\u5197\u4f59\u8bbe\u8ba1\u6709\u5229\u4e8e\u63d0\u9ad8\u8f7d\u4eba\u822a\u5929\u5668\u6c14\u4f53\u76d1\u63a7\u7684\u5b89\u5168\u6027\u548c\u53ef\u9760\u6027\u3002\u822a\u5929\u5458\u51fa\u8231\u6d3b\u52a8\u662f\u8f7d\u4eba\u822a\u5929\u7684\u91cd\u8981\u4efb\u52a1\u4e4b\u4e00\u3002\u822a\u5929\u5458\u592a\u7a7a\u884c\u8d70\u65f6,\u8231\u5916\u822a\u5929\u670d(EMU)\u53d1\u52a8\u673a\u5c06\u4ea7\u751f\u6709\u6bd2\u7684\u80bc\u7c7b\u7269\u8d28,\u5e76\u5438\u9644\u5728\u8231\u5916\u822a\u5929\u670d\u4e0a,\u884c\u8d70\u5b8c\u6210\u540e\u88ab\u5e26\u56de\u8231\u5185,\u800c\u80bc\u7c7b\u7269\u8d28\u68c0\u6d4b\u5e38\u7528\u9635\u5217\u8d28\u8c31\u4eea\u3002\u53e6\u5916,\u5c06\u5c0f\u578b\u9635\u5217\u8d28\u8c31\u4eea\u7528\u4e8e\u8231\u5916\u4fbf\u643a\u5f0f\u751f\u547d\u4fdd\u969c\u7cfb\u7edf,\u53ef\u5927\u5927\u964d\u4f4e\u4fbf\u643a\u5f0f\u751f\u547d\u4fdd\u969c\u7cfb\u7edf\u7684\u8d28\u91cf\u3001\u4f53\u79ef\u548c\u529f\u8017,\u51cf\u8f7b\u8231\u5916\u822a\u5929\u670d\u8d1f\u8377,\u63d0\u9ad8\u822a\u5929\u5458\u592a\u7a7a\u884c\u8d70\u7684\u81ea\u7531\u673a\u52a8\u6027\u3002\u5e76\u4e14\u53ef\u4ee5\u5b9e\u73b0\u5b9e\u65f6\u68c0\u6d4b,\u663e\u793a\u822a\u5929\u5458\u7684\u5b89\u5168\u7b49\u7ea7,\u53ca\u65f6\u62a5\u77e5\u6f5c\u5728\u5371\u9669,\u63d0\u9ad8\u51fa\u8231\u6d3b\u52a8\u7684\u5b89\u5168\u53ef\u9760\u6027\u3002\u6b64\u5916,\u5b83\u8fd8\u53ef\u7528\u4f5c\u8231\u5916\u6b8b\u4f59\u6c14\u4f53\u5206\u6790\u5668,\u5b9a\u6027\u5b9a\u91cf\u76d1\u6d4b\u6c28\u3001\u706b\u7bad\u63a8\u8fdb\u5242\u3001\u6c27\u3001\u6c2e\u548c\u6c34\u7684\u8231\u5916\u6cc4\u6f0f\u3002\u5c0f\u578b\u9635\u5217\u8d28\u8c31\u4eea\u7684\u8231\u5916\u5e94\u7528\u5df2\u57282001\u5e742\u6708\u7531\u4e9a\u7279\u5170\u8482\u65af\u822a\u5929\u98de\u673a\u8fd0\u5f80\u56fd\u9645\u7a7a\u95f4\u7ad9\u5f00\u59cb\u5e94\u7528\u3002<\/p>\n

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2.13 \u5211\u4e8b\u79d1\u6280<\/strong><\/p>\n

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\"\"<\/p>\n

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