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\uff082\uff09\u7814\u7a76\u7535\u5bfc\u7387\u7684\u53d8\u5316<\/strong><\/p>\n

\u5728\u592a\u9633\u80fd\u7535\u6c60\u5236\u5907\u4e2d\uff0c\u901a\u5e38\u5728ITO \u4e0e\u6d3b\u6027\u5c42\u4e2d\u95f4\u63d2\u5165PEDOT:PSS \u4f5c\u4e3a\u7a7a\u7a74\u4f20\u8f93\u5c42\u3002\u5728PEDOT:PSS \u6c34\u6eb6\u6db2\u4e2d\uff0cPEDOT\u548cPSS \u5f62\u6210\u4e00\u79cd\u80f6\u675f\u7ed3\u6784\u3002\u5e94\u7528\u65f6\uff0c\u5bf9PEDOT:PSS \u8584\u819c\u8fdb\u884c\u4e86\u4e0d\u540c\u65f6\u95f4\u7684\u7d2b\u5916\u81ed\u6c27\u5904\u7406\uff0c\u5229\u7528\u626b\u63cf\u63a2\u9488\u663e\u5fae\u955cSPM \u5bf9\u8584\u819c\u7684\u8868\u9762\u5f62\u8c8c\u548c\u7535\u5bfc\u7387\u7684\u53d8\u5316\u8fdb\u884c\u7814\u7a76\uff0c\u5e76\u901a\u8fc7\u5236\u5907\u7ecf\u5178\u6709\u673a\u592a\u9633\u80fd\u7535\u6c60\u5668\u4ef6\u7684\u6027\u80fd\u6d4b\u8bd5\u6765\u5370\u8bc1\u8fd9\u4e9b\u53d8\u5316\u89c4\u5f8b\uff0c\u4ece\u800c\u8fbe\u5230\u4f18\u5316\u7535\u6c60\u5668\u4ef6\u7684\u76ee\u7684\u3002<\/p>\n

2\u3001\u5bfc\u7535\u805a\u5408\u7269\u4e2d\u7684\u5e94\u7528<\/strong><\/p>\n

\u626b\u63cf\u63a2\u9488\u663e\u5fae\u955c(SPM)\u56e0\u5176\u5177\u6709\u5206\u8fa8\u7387\u9ad8(\u53ef\u8fbe\u539f\u5b50\u6c34\u5e73\u5206\u8fa8\u7387)\u3001\u6837\u54c1\u51c6\u5907\u7b80\u5355\u3001\u53d7\u5de5\u4f5c\u73af\u5883\u9650\u5236\u5c11\u3001\u529f\u80fd\u591a\u6837\u5316(\u5177\u6709\u591a\u79cd\u64cd\u4f5c\u6a21\u5f0f)\u7b49\u4f18\u70b9\uff0c\u5229\u7528\u5fae\u5c0f\u7684\u63a2\u9488\u626b\u63cf\u6837\u54c1\u7684\u8868\u9762\u4ee5\u83b7\u5f97\u6837\u54c1\u8868\u9762\u5f62\u8c8c\u7279\u5f81\u4ee5\u53ca\u63a2\u9488\u4e0e\u6837\u54c1\u76f8\u4e92\u4f5c\u7528\u7684\u4fe1\u606f\u3002SPM\u4e0d\u4ec5\u80fd\u591f\u89c2\u5bdf\u6837\u54c1\u7684\u8868\u9762\u5f62\u8c8c,\u4e5f\u80fd\u6d4b\u91cf\u5fae\u89c2\u5c3a\u5bf8 \u4e0b\u6750\u6599\u7684\u5404\u79cd\u6027\u8d28,\u5e76\u5177\u6709\u7eb3\u7c73\u52a0\u5de5\u7684\u529f\u80fd\u3002
\n \u00a0\uff081 \uff09\u5bfc\u7535\u805a\u5408\u7269\u8584\u819c\u8868\u9762\u5f62\u8c8c\u548c\u7ed3\u6784\u7684\u7814\u7a76<\/strong><\/p>\n

\u5bfc\u7535\u805a\u5408\u7269\u901a\u5e38\u662f\u901a\u8fc7\u7535\u5316\u5b66\u805a\u5408\u7684\u65b9\u6cd5\u5728\u7535\u6781\u4e0a\u5f62\u6210\u8584\u819c\u6216\u7528\u6eb6\u6db2\u65cb\u6d82\u7684\u65b9\u6cd5\u5728\u57fa\u5e95\u4e0a\u5f62\u6210\u8584\u819c\u3002\u7528STM\u548cAFM\u5bf9\u8584\u819c\u7684\u8868\u9762\u5f62\u8c8c\u7684\u89c2\u5bdf\u548c\u5fae\u89c2\u7ed3\u6784\u7684\u8868\u5f81\u5177\u6709\u5341\u5206\u91cd\u8981\u7684\u610f\u4e49\u3002\u5728\u4e09\u7ef4\u751f\u957f\u4e2d,\u5728\u5e73\u884c\u548c\u5782\u76f4\u4e8e\u7535\u6781\u8868\u9762\u7684\u65b9\u5411\u4e0a\u6838\u7684\u751f\u957f\u901f\u7387\u51e0\u4e4e\u76f8 \u540c\u3002\u4f46\u5728\u4e8c\u7ef4\u751f\u957f\u8fc7\u7a0b\u4e2d,\u5728\u5e73\u884c\u4e8e\u7535\u6781\u8868\u9762\u65b9\u5411\u4e0a\u7684\u6838\u7684\u751f\u957f\u901f\u7387\u6bd4\u5782\u76f4\u4e8e\u7535\u6781\u8868\u9762\u65b9\u5411\u4e0a\u7684\u5feb\u5f97\u591a\u3002\u7531\u4e0b\u56fe\u53ef\u770b\u51fa\uff0c\u5f53\u805a\u5408\u65f6\u95f4\u4e3a01025s\u65f6\u6cbf\u57fa\u5e95\u65b9\u5411\u7684\u751f\u957f\u901f\u5ea6\u5feb\u4e8e\u5782\u76f4\u4e8e\u57fa\u5e95\u7684\u65b9\u5411,\u800c\u4e14\u751f\u957f\u6838\u7684\u6570\u76ee\u8f83\u5c11;\u7136\u800c\u5f53\u805a\u5408\u65f6\u95f4\u589e\u52a0\u523001050s\u65f6,\u5e73\u884c\u4e8e\u548c\u5782\u76f4\u4e8e\u57fa\u5e95\u8868\u9762\u65b9\u5411\u4e0a\u7684\u751f\u957f\u901f\u5ea6\u76f8\u5dee\u4e0d\u591a\u5e76\u4e14\u751f\u957f\u6838\u7684\u6570\u76ee\u5927\u5927\u5730\u589e\u52a0\u4e86\u3002\u56e0\u6b64\u8584\u819c\u5728\u805a\u5408\u65f6\u95f4\u4e3a01025s\u65f6\u662f\u4e8c\u7ef4\u77ac\u65f6\u751f\u957f,\u5f53\u805a\u5408\u65f6\u95f4\u589e\u52a0\u523001050s\u65f6\u662f\u4e09\u7ef4\u6e10\u8fdb\u751f\u957f\u3002\u805a\u82ef\u80fa\u3001\u805a\u5421\u54af\u7b49\u5bfc\u7535\u805a\u5408\u7269,\u53ef\u7528\u4f5c\u8461\u8404\u7cd6\u6c27\u5316\u9176 \u7684\u56fa\u5b9a\u3002\u901a\u8fc7STM\u5bf9\u8868\u9762\u5f62\u8c8c\u8fdb\u884c\u89c2\u5bdf\u53ef\u4ee5\u786e\u5b9a\u8461\u8404\u7cd6\u6c27\u5316\u9176\u662f\u5426\u88ab\u56fa\u5b9a\u5230\u4e86\u5bfc\u7535\u805a\u5408\u7269\u8584\u819c\u4e0a\u3002<\/p>\n

\"\"<\/p>\n

\u56fe3 \u00a0AFM\u56fe\u8c61\u5206\u6790<\/strong><\/p>\n

\u53e6\u5916\uff0c\u5bf9\u8584\u819c\u8868\u9762\u5f62\u8c8c\u7684\u5f71\u54cd\u53ef\u7528\u539f\u4f4d\u7535\u5316\u5b66\u539f\u5b50\u529b\u663e\u5fae\u955c(insituEC-AFM)\u8fdb\u884c\u7814\u7a76\u3002<\/p>\n

\uff082\uff09\u5bfc\u7535\u805a\u5408\u7269\u7684\u7eb3\u7c73\u52a0\u5de5<\/strong><\/p>\n

\u968f\u7740SPM\u548c\u7eb3\u7c73\u6280\u672f\u7684\u53d1\u5c55,SPM\u7684\u63a2\u9488\u53ef\u4ee5\u7528\u6765\u5728\u57fa\u5e95\u8868\u9762\u4e0a\u8bf1\u5bfc\u5bfc\u7535\u805a\u5408\u7269\u7684\u805a\u5408\u6216\u7528\u5bfc\u7535\u805a\u5408\u7269\u5bf9\u57fa\u5e95\u8868\u9762\u8fdb\u884c\u4fee\u9970\u3002STM\u8f85\u52a9\u7684\u5bfc\u7535\u805a\u5408\u7269\u7535\u805a\u5408\u8fc7\u7a0b\u662f\u901a\u8fc7STM\u7684\u9488\u5c16\u4e3a\u5728\u6240\u9009\u62e9\u7684\u8868\u9762\u533a\u57df\u8fdb\u884c\u5c40\u90e8\u7535\u805a\u5408\u63d0\u4f9b\u6240\u9700\u7684\u9a71\u52a8\u529b\u3002AFM\u8f85\u52a9\u7684\u5c40\u90e8\u7535\u805a\u5408\u548c\u8868\u9762\u4fee\u9970\u662f\u7531\u626b\u63cf\u7740\u7684\u6216\u5171\u632f\u7684AFM\u63a2\u9488\u63d0\u4f9b\u7684\u6c34\u5e73\u522e\u64e6\u529b\u548c\u5782\u76f4\u6572\u51fb\u529b\u4f5c\u4e3a\u9a71\u52a8\u529b,\u4ece\u800c\u4f7f\u5bfc\u7535\u805a\u5408\u7269\u5355\u4f53\u5728\u57fa\u5e95\u4e0a\u8fdb\u884c\u5c40\u90e8\u9009\u62e9\u6027\u7535\u805a\u5408\u6216\u7528\u5bfc\u7535\u805a\u5408\u7269\u5728\u57fa\u5e95\u4e0a\u8fdb\u884c\u7eb3\u7c73\u56fe\u6848\u5316\u4fee\u9970\u3002AFM\u8fd8\u53ef\u4ee5\u7528\u6765\u5bf9\u5bfc\u7535\u805a\u5408\u7269\u5206\u5b50\u94fe\u8fdb\u884c\u642c\u8fd0\u548c\u5207\u5272\u3002\u6bd4\u5982Ito\u7b49\u4eba\u6700\u521d\u7528STM\u5728\u4f4e\u6e29\u4e0b(\u4f4e\u4e8e275K)\u89c2\u5bdf\u5230\u4e86HOPG\u57fa\u5e95\u4e0a\u805a\u82ef\u80fa\u548cB-\u73af\u7cca\u7cbe\u5f62\u6210\u7684\u68d2\u72b6\u5305\u7edc\u7269(InclusionComplex)\u7684\u7edd\u7f18\u5206\u5b50\u5bfc\u7ebf,\u540e\u6765\u53c8\u7528AFM\u5728\u5ba4\u6e29\u4e0b\u89c2\u5bdf\u5230\u4e86\u4e91\u6bcd\u57fa\u5e95\u4e0a\u805a\u82ef\u80fa\u548c\u7531A-\u73af\u7cca\u7cbe\u5408\u6210\u7684\u5206\u5b50\u7eb3\u7c73\u7ba1\u4e4b\u95f4\u5f62\u6210\u7684\u68d2\u72b6\u5305\u7edc\u7269\u7edd\u7f18\u5206\u5b50\u5bfc\u7ebf\u3002<\/p>\n

\uff083\uff09\u5bfc\u7535\u805a\u5408\u7269\u8868\u9762\u7684\u7535\u5b66\u6027\u8d28<\/strong><\/p>\n

\u7531\u4e8e\u5177\u6709\u975e\u5e38\u5c0f\u7684\u9488\u5c16\u5c3a\u5bf8,\u626b\u63cf\u63a2\u9488\u663e\u5fae\u955c\u4e5f\u662f\u4e00\u79cd\u7814\u7a76\u5bfc\u7535\u805a\u5408\u7269\u5c40\u90e8\u7535\u5b66\u6027\u8d28\u7684\u7406\u60f3\u5de5\u5177\u3002\u5c06STM\u548cAFM\u76f8\u7ed3\u5408\u5bf9\u63ba\u6742\u7684\u805a\u5421\u54af\u6837\u54c1\u8fdb\u884c\u7814\u7a76\u65f6,\u5728\u626b\u63cf\u6837\u54c1\u8868\u9762\u5f62\u8c8c\u7684\u8fc7\u7a0b\u4e2d\u540c\u65f6\u5f97\u5230\u4e86\u53cd\u6620\u6837\u54c1\u8868\u9762\u4e0d\u540c\u533a\u57df\u5bfc\u7535\u6027\u80fd\u7684\u7535\u6d41\u56fe,\u89c2\u5bdf\u5230\u6837\u54c1\u8868\u9762\u5b58\u5728\u5177\u6709\u4e0d\u540c\u5bfc\u7535\u6027\u80fd\u7684\u533a\u57df\u3002\u6b64\u5916,\u9759\u7535\u529b\u663e\u5fae\u955c(electrostaticforcemicroscopy,EFM)\u4e5f\u53ef\u4ee5\u7528\u6765\u8868\u5f81\u5bfc\u7535\u805a\u5408\u7269\u7684\u7535\u5b66\u6027\u8d28\u3002<\/p>\n

\uff084\uff09\u539f\u4f4d\u7814\u7a76\u5bfc\u7535\u805a\u5408\u7269\u8584\u819c\u539a\u5ea6\u7684\u53d8\u5316<\/strong><\/p>\n

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\u53c2\u8003\u6587\u732e\uff1a<\/b><\/strong><\/p>\n

[1] \u90ed\u654f\u6960. \u626b\u63cf\u63a2\u9488\u663e\u5fae\u955c\u5728\u6709\u673a\u592a\u9633\u80fd\u7535\u6c60\u7814\u7a76\u4e2d\u7684\u5e94\u7528[D]. \u5929\u6d25:\u5929\u6d25\u7406\u5de5\u5927\u5b66, 2016. 14-18<\/p>\n

[2] \u6768\u6d9b, \u725b\u5229, \u674e\u58ee. \u626b\u63cf\u63a2\u9488\u663e\u5fae\u955c\u5728\u5bfc\u7535\u805a\u5408\u7269\u7814\u7a76\u4e2d\u7684\u5e94\u7528[J]. \u5e94\u7528\u5316\u5b66, 2006, 23(2): 1-3<\/p>\n

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